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《Journal of Analytical Science》 2014-04
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Determination of 4-Hydroxycarbazole by Brij35 Micellar Enhanced Spectrofluorometry

ZHANG Hai-rong;YAN Jing-jing;CHEN Jin-e;Research Institute of Biochemistry Analysis,Xinzhou Teachers University;  
The effects of reaction time,metal ions and pH on the fluorescence properties of 4-hydroxycarbazole in different media such as water,ethanol,methanol,SDS,β-CD,CTMAB and Brij35 were investigated by spectrofluorometry.The results suggested that the fluorescence intensity of 4-hydroxycarbazole was greatly enhanced in Brij35 solution with a strong peak atλex/λem = 337/357 nm.A method for the determination of 4-hydroxycarbazole by Brij35 micellar enhanced spectrofluorometry was developed.The linear range of this method was 4.0×10-7-1.0×10-4 mol/L with the detection limit of 6.5×10-8 mol/L and RSD of 2.91%.
【Fund】: 忻州师范学院应用化学创新实践基地项目(2013-31);; 山西省教育厅强校工程项目(J2012092);; 忻州师范学院科研基金(2011052);; 山西省忻州市科技研发项目(忻科发No.201231-20)
【CateGory Index】: X832;O657.3
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