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《Analytical Laboratory》 2003-03
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Flow injection with electrothermal atomic absorption spectrometry for determination of gold, platinum and palladium in geochemical samples

LI Zhong-xi and ZHOU Li-ping(Northwest Non-ferrous Geological Research Institute, Xi′an 710054)  
A flow injection on-line per-concentration system was coupled with electrothermal atomic absorption spectrometry for the determination of trace gold, platinum, palladium in geochemical samples. The system was investigated and the experimental conditions were optimized. The enrichment factors for Au, Pt, Pd were 43, 37, 41, respectively. The detection limit(3σ) for Au, Pt, Pd were 5, 16, 9 ng/L, respectively. The RSD of Au, Pt, Pd were 3.6%, 5.1%, 4.7%, respectively. Using the established method, the contents of Au, Pt, Pd in four standard reference materials were determined and the results were found to be in good agreement with the reference values.
【CateGory Index】: O657.31
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