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《Analytical Laboratory》 2004-03
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Kinetic spectrophotometry for the determiantion of trace vanadium(Ⅴ) by azocarmine B-(KBrO_3) system

LI Zu-bi~*, LI Chong-ning, WANG Jia-lin (Adult Education College, Yunnan University) and CAO Qiu-e (Department of Chemistry, Yunnan University, Kunming 650091),Fenxi Shiyanshi,2004,23(3):22~24  
The oxidation reaction of azocarmine B (AZB) by KBrO_3 can be catalyzed by vanadium(Ⅴ) in the (presence) of ascorbic acid as activator. Based on this, a new kinetic spectrophotometry for the determination of trace V(Ⅴ) was established. Under the optimum reaction conditions and kinetic parameters, the linear range for the determination of V(Ⅴ) was 1.0~3.2 ng/mL with the detection limit of 1.1×10~(-2) ng/mL. The relative standard deviation for 10 replicate determinations of 2 ng/mL V(Ⅴ) was calculated to be 0.20%. The results indicated that many common ions did not interfere in the determination. The method was used for the determination of trace vanadium in coptis, tea, rice and flour samples with the relative standard deviation over 2.7%~3.9% and the recovery over 97.1%~105.4%.
【CateGory Index】: O657.32
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