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《Analytical Laboratory》 2004-04
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Determination of residual solvents content(hexane residue) in plant oil by headspace solid-phase microextraction

LAN Fang, XIE Liqi, YANG Zuo-jun~*, PAN Kun-yong (Shenzhen Entry-Exit Inspection and Quarantine Bureau of the People′s Republic of China, Shenzhen 518045) and WU Cai-ying (Wuhan University, Wuhan 430072)  
The headspace solid-phase microextraction(HS-SPME) with a novel fiber coated with sol-gel fullerene coupled with gas chromatography-flame detector(GC-FID) was used to determine the primary residual solvent, hexane in plant oil. The variable factors affecting the SPME absorption and desorption process were optimized. Estimated detection limits of the method for the residual solvent, hexane in plant oil was 1.47 μg/kg(S/N=5) with RSD of 1.9%( n =7) and recovery of 88.4%~102.1%. The sensitivity of the method was 100 times sensitive than that of GB/T5009.37-1996.
【Fund】: 国家检验检疫局科研项目(K032 1999)
【CateGory Index】: O657.7
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【References】
Chinese Journal Full-text Database 7 Hits
1 Fu Ruo-nong(Department of Chemistry Beijing Institute of Technoligy, Beijing 100081);Advances on gas chromatography in China in recent two years(Ⅱ)[J];Analytical Laboratory;2005-05
2 Fu Zhonghua1,Ren hongbo2 (1.Henan jingu Industray Development CO.,LTD,Zhengzhou 450053,China 2.Heilongjiang Academy of Agricultural Sciences,Heilongjiang 150086,China);Determination of 6# Solvent Residue in Vegetable Oil by Head-Space GC[J];Grain Distribution Technology;2010-04
3 MA Jun-gang;DING Chun-rui;JIAN Li-jun;Xinjiang product quality supervision and inspection research institute;;Determination of solvent residue in vegetable oils by headspace gas chromatography[J];Food Engineering;2013-04
4 LIU Xiao-jun1,2,JIN Qing-zhe1,2,WANG Shan-shan3,LIU Yuan-fa1,2,WANG Xing-guo*1,2(1.State Key Laboratory of Food Science and Technology,Jiangnan University,Wuxi 214122,China;2.School of Food Science and Technology,Jiangnan University,Wuxi 214122,China;3.Shandong Luhua Group Co.,Ltd,Laiyang 265200,China);Optimazation of Solid-Phase Microextraction Conditions Combined with GC-MS for Analysis of Volatiles in Peanut Oil[J];Journal of Food Science and Biotechnology;2010-04
5 SHENTU Xian-yan,ZHANG Wen(Zhejiang Transfar Co.,Ltd.,Hangzhou 311215,China);Determination of residual acrylate monomers in the coatings[J];Dyeing & Finishing;2008-05
6 LU Hao,BI Yanlan,ZHAO Ziwei,YANG Huifang,WANG Menghua(Faculty of Food Science and Engineering,Henan University of Technology,Zhengzhou 450052,China);Status of oil detection technology[J];China Oils and Fats;2009-04
7 WU Cui-rong1,2,SUN Nan1,CHAI Zhen-lin2,YANG Liu2,ZHU Jie-li2(1 Zhejiang University of Technology,Hangzhou 310014,China;2.Zhejiang Forest Product Quality Testing Station,Hangzhou 310023,China);Application of SPME in Analysis of Edible Vegetable Oil[J];Journal of Zhejiang Forestry Science and Technology;2013-03
【Co-citations】
Chinese Journal Full-text Database 10 Hits
1 ZHANG Xiao-yong~1,HUANG Wei~2,SI Wei~3,LU Feng~4,WANG Zhen-hong~5(1.2.3.4 Jiangsu Environmental Monitoring Center,Nanjing?210036,China;5.Department of Chemistry and Environment Science,Zhangzhou Normal University,Zhangzhou?363000,China);Control and Actuality of the Air Pollution Indoor[J];Environmental Science and Management;2006-06
2 YU Hai-xia(Wenzhou Water Quality Laboratory of Wenzhou Water Group Corporation,Wenzhou 325027,China);Determination of Trihalomethane in Water by Purge and Trap-Gas Chromatography[J];Analysis and Testing Technology and Instruments;2008-02
3 FU Ruo nong (Department of Chemistry, Beijing Institute of Technology, Beijing 100088),Fenxi Shiyanshi,2003,22(2):94~107;Advances on gas chromatography in China[J];Analytical Laboratory;2003-02
4 QU Gang-lian,MA Guo-hua,PAN Rong-rong and LI Fen-run(Analytical Center,Institute of Chemical Defence,Beijing 102205);Study of compound independent calibration by GC-AES[J];Chinese Journal of Analysis Laboratory;2007-11
5 Liu Jie, Liu Jun, Jia Ke, Xu Dong, Wang Miao, Bo Xue dong (Lunan Pharmaceutical Co., Ltd., Linyi, 276000);Determination of nine solvent residues in epirubicin hydrochloride by head-space gas chromatography[J];Analytical Instrumentation;2010-03
6 FU Xiao-chun(Urumqi Environmental Monitoring Center,Urumqi Xinjiang 830000,China);Determination of Volatility Organic Compounds(VOCs) in Water by Purge and Trap-gas Chromatography[J];Arid Environmental Monitoring;2009-04
7 QU Bai-lu,XU Xiong-fei,CHEN Jun(Chang Sha Environmental and Monitoring Central Station,Changsha 410001,China);Determination of 26 Kinds of Volatile Organic Compounds in Water by Purge-trap and GC-MS[J];Guangzhou Chemistry;2010-04
8 Yang Xia Song Dajun (Shandong Kaitai Company Limited, Zibo 255040, China) (Shandong Institute of Chemical Industry, Jinan 250014, China);INCREASING ACRYLONITRILE ANALYSIS SPEED BY MULTI-DIMENSIONAL GAS CHROMATOGRAPHY[J];Chemical Analysis and Meterage;2007-06
9 PAN Rong-rong,QU Gang-lian,MA Guo-hua,LI Fen-run(Analysis Center,Institute of Chemical Defense,Beijing 102205,China);Determination of systemic poisons by CIC method of GC-AED[J];Chemical Engineer;2007-02
10 FU Ruo-nong (Department of Chemistry,Beijing Institute of Technology,Beijing 100081,China);The evolution and advances of solid-phase microextraction[J];Chemical Reagents;2008-01
【Co-references】
Chinese Journal Full-text Database 10 Hits
1 LI Na et al(College of Life and Environmental Science,Minzu University of China,Beijing 100081);Research Progress on Solvent Extraction of Vegetable Oil[J];Journal of Anhui Agricultural Sciences;2012-06
2 WU Xiao Ying,TONG Cheng Ling,ZHONG Huai Bin (Anhui Provincial Institute for Drug Control,Hefei 230061);Determination of residual organic solvents in rifaximin by GC[J];Anhui Medical and Pharmaceutical Journal;2004-02
3 GU Hong( Dept of Chemical Engineering of Yancheng Institute of Technology,Yancheng 224003,China);Determination of the organic solvent residue in raloxifence by GC[J];Anhui Medical and Pharmaceutical Journal;2004-04
4 TAO Jing (Department of Chemistry,Anshan Normal University,Anshan Liaoning 114005,China);Research of Benzoyl Peroxide in Flour by Gas Chromatography[J];Journal of Anshan Normal University;2004-02
5 XU Hua 1 YI Rong 2 CHEN Da-zhou 2 LI Lei 1 (1.College of Science, Beijing University of Chemical Technology, Beijing 100029; 2.National Research Center of Certified Reference Material, Beijing 100013, China);Pretreatment for determination of PCBs in fish oil by GC/MS[J];Journal of Beijing University of Chemical Technology;2003-05
6 Liu Yizi Xie Mengxia Han Jie Liu Yuan Qiu Yueming Ding Yayun Zhang Lei (Analytical and Testing Center, Beijing Normal University, 100875, Beijing, China);DETERMINATION OF CHLORAMPHENICOL RESIDUE IN HONEY BY COUPLING SOLID-PHASE EXTRACTION WITH GAS CHROMATOGRAPHY-MASS SPECTROMETRY[J];Journal of Beijing Normal University(Natural Science);2004-02
7 XU Fang1,LU Li-xin1,2(1.Jiangnan University,Wuxi 214122,China;2.National Light Industry Package Quality Supervising and Testing Center,Wuxi 214122,China);Research Progress on the Oil Anti-oxidation Mechanism and Anti-oxidation Packaging of Fatty Food[J];Packaging Engineering;2008-06
8 ZHANG Min,QI Jin-gang,LIU Bao-yuan,YANG Yi-gang(Department of Physics,Changchun Normal University,Changchun 130032,China);The Fast Detect Instrument of Corn Oil Quality Based on TMS320VC6412[J];Journal of Changchun Normal University;2006-02
9 HAI Zheng, WANG Jun (College of Biosystems Engineering and Food Science, Zhejiang University, Hangzhou 310029, China);Studies on Signal Feature Extraction and Sensor Optimization of an Electronic Nose[J];Chinese Journal of Sensors and Actuators;2006-03
10 YU Qian~1,LAI Zi-ni~2,FU Lian-jin~3,ZHENG Wen-hui~4,FU Min-zhi~5,ZHAO Zhi-feng~1, (1.College of Chemical Engneering and Light Industry, Guangdong University of Technology, Guangzhou 510090,China;2.Pearl River Fisheries Research Institute CAFS,Guangzhou 510380,China; 3.Guangdong Huizhou Quality & Measuring Testing Institute,Huizhou 516002,China;4.Zhongshan University, Guangzhou 510060,China;5.Yangchun Enviromental Monitoring Station,Yangchun 529600,China.);Abstraction and Determination of Methyl Mercury in Fish[J];Urban Environment & Urban Ecology;2004-04
【Secondary References】
Chinese Journal Full-text Database 10 Hits
1 LIU Hai-cang1,TENG Zhao-sheng1,LIU Jing-bo2,XIONG Hai-tao1,LUO Bin1(1.School of Electrical and Information Engineering,Hunan University,Changsha 410082,China; 2.Changsha High-tech Development Zone,YiQi Measurement and Control Technology Corporation, Changsha 410082,China);Design of digital sensor for oil quality detection based on AD7745[J];Transducer and Microsystem Technologies;2011-09
2 GONG Hong-wei1,2,YANG Xiao-hong,1,CHEN Di1,DONG Lei1,SUN Hao3(1.School of Pharmaceutical Sciences,Jilin University,Changchun 130021,China;2.School of Public Health,Jilin University,Changchun 130021,China;3.Faculty of Chemistry,Northeast Normal University,Changchun 130024,China);Chemical constituents of volatile oil from leaf of Prunus tomentosa Thunb[J];Journal of Molecular Science;2008-04
3 LIANG Hui1,LU Bin-bin2,LU Qi-yu1,ZHANG Shao-bing1(1.College of Grain,Oil and Food,Henan University of Technology,Zhengzhou 450001,China)(2.Zhengzhou Tobacco Research Institute,Zhengzhou 450001,China);Study on Extraction Volatiles in Peanut Oil by SDE[J];Modern Food Science and Technology;2013-03
4 Yu Xiuzhu1Yang Chen1Du Shuangkui1Gao Jinming2(1.College of Food Science and Engineering,Northwest A &F University,Yangling,Shaanxi 712100,China 2.College of Science,Northwest A &F University,Yangling,Shaanxi 712100,China);Determination of Acid Value of Edible Oils Based on Electrical Conductivity Change Value of Alkaline Solution during Reaction[J];Transactions of the Chinese Society for Agricultural Machinery;2011-09
5 LIU Li-ting1,*GE Wu-peng1,CHEN Ying2,YANG Jing3,WANG Qian3,CAO Ni-na3(1.College of Food Science and Engineering,Northwest A&F University,Yangling,Shaanxi 712100,China; 2.Information Center of Shaanxi Bureau of Quality and Supervision,Xi'an,Shaanxi 710006,China; 3.Institution of Inspection of Yangling Bureau of Quality and Supervision,Yangling,Shaanxi 712100,China);Research Progress on Different Inspections of Drainage Oils[J];Academic Periodical of Farm Products Processing;2012-09
6 BAO Zhi-hua1,ZHANG Wen-hui2(1.Inner Mongolia Business Vocational Collage,Huhhot 010070,China; 2.Huhhot Center for Disease Control and Prevention,Huhhot 010070,China);HEADSPACE CAPILLARY GAS CHROMATOGRAPHY METHOD FOR AUTOMATIC DETERMINATION OF RESIDUAL SOLVENTS IN EDIBLE VEGETABLE OILS[J];Journal of Inner Mongolia Agricultural University(Natural Science Edition);2012-04
7 LENG Baizhong 1 , JIA Yanling 2 (1. Changtu Grain Quality Supervision Station of Liaoning Province, Tieling Liaoning 112500, China; 2. Siping Branch of Hunan Zhenghong Tech Firm, Siping Jilin 136001, China);Determination of Residual Solvent in Edible Vegetable Oil with Ggas Chromatographic Method[J];Agricultural Science & Technology and Equipment;2013-02
8 Zhang Kun Zhang Hua(Bazhong Grain Quality Supervision and Inspection Station 636000);SELECTION OF STANDARD RESIDUE SOLVENTIN EDIBLE VEGETABLE OIL[J];Grain Storage;2013-02
9 Ni Xiaoying;Qin Shimin;Huang Li;Mei Guang;Yang Jing;Shen Na;Hunan State Grain Quality Monitoring Center;Hunan Province Grain Science Research and Design Institute;;Overview of Rapid Identification Methods on Drainage Oils[J];Grain Science and Technology and Economy;2014-02
10 GAN Yunjuan TANG Ying GUO Chunmei TAN Hui (Hainan Provincial Quality Monitoring Center for Grain and Oil Products,Haikou,Hainan 570203);Detection of Residual Solvent and Equilibrium Conditions of Edible Vegetable Oil Using Headspace Gas Chromatography[J];Tropical Agricultural Engineering;2010-01
【Secondary Citations】
Chinese Journal Full-text Database 5 Hits
1 Chen Wenrui, Guo Changcheng Liu Guochang (The National Import Food Hygiene Supervision and Inspection Center of China, Guangzhou 510405);Determination of Trace Xylene in Contaminated Palm Oil by Soh'd Phase Micro-extraction and Capillary Gas Chromatography[J];Chinese Journal of Analytical Chemistry;1999-06
2 Liu Jiyan, Jiang Guibin (Research Centre for Eco-Environmental Sciences, Chinese Academy of Sciences, Beijing 100085);Application of Solid Phase Microextraction to Analysis of Organotin and Organomercury Compounds[J];Chinese Journal of Analytical Chemistry;1999-10
3 Fang Ruibin and Zhang Shihong(Chem. Dept. of Yunnan University, Kunming, 650091);SUPERCRITICAL FLUID CO_2 EXTRACTION OF COLCHICINE FROM COLCHICINE AUTUMNELE LILIACEAE[J];Chinese Journal of Chromatography;1999-03
4 Wang Zhenyu(Department Of Chemistry, Wuhan University, Wuhan, 430072);A Novel Solid Phase Coating of Solid-Phase Microextraction Prepared with Sol-Gel Technology and its Applications[J];Chinese Journal of Chromatography;1999-03
5 Zhang Daoning, Wu Caiying and Ai Fei (Department of Chemistry, Wuhan University, Wuhan, 430072);Research of Polymer Coating in Solid Phase Microextraction[J];CHINESE JOURNAL OF CHROMATOGRAPHY;1999-01
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