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《Chinese Journal of Analysis Laboratory》 2008-04
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Determination of organochlorine and pyrethroid pesticides in vegetable samples by ultrasonic extraction and SPME-GC method

ZHANG Mao-sheng1,2,GONG Li-fen1,3,YU Bin-bin1,ZENG Jing-bin1,YUAN Ning1 and CHEN Xi*1(1.Department of Chemistry and the Key Laboratory of Analytical Sciences of the Ministry of Education,College of Chemistry and Chemical Engineering,Xiamen University,Xiamen 361005;2.Department of Chemistry and Environmental Science,Zhangzhou Normal University,Zhangzhou 363000;3.School of Chemistry and Life Science,Quanzhou Normal University, Quanzhou 326000)  
A new method used for the determination of organochlorine and pyrethroid pesticides from vegetable samples coupling ultrasonic extraction with SPME-GC is presented here.The experimental conditions were also controlled and optimised.It is showed that the residues and pigments,who can effect greatly the experimental results,were avoided by dilution.We also demonstrated the practical applicability of this method.
【Fund】: 福建省科技计划(2005I-030 2006Y0026);; 福建省教育厅科技(JA07156)项目资助
【CateGory Index】: TS255.7
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