Full-Text Search:
Home|Journal Papers|About CNKI|User Service|FAQ|Contact Us|中文
《Chinese Journal of Analysis Laboratory》 2008-04
Add to Favorite Get Latest Update

Determination of organochlorine and pyrethroid pesticides in vegetable samples by ultrasonic extraction and SPME-GC method

ZHANG Mao-sheng1,2,GONG Li-fen1,3,YU Bin-bin1,ZENG Jing-bin1,YUAN Ning1 and CHEN Xi*1(1.Department of Chemistry and the Key Laboratory of Analytical Sciences of the Ministry of Education,College of Chemistry and Chemical Engineering,Xiamen University,Xiamen 361005;2.Department of Chemistry and Environmental Science,Zhangzhou Normal University,Zhangzhou 363000;3.School of Chemistry and Life Science,Quanzhou Normal University, Quanzhou 326000)  
A new method used for the determination of organochlorine and pyrethroid pesticides from vegetable samples coupling ultrasonic extraction with SPME-GC is presented here.The experimental conditions were also controlled and optimised.It is showed that the residues and pigments,who can effect greatly the experimental results,were avoided by dilution.We also demonstrated the practical applicability of this method.
【Fund】: 福建省科技计划(2005I-030 2006Y0026);; 福建省教育厅科技(JA07156)项目资助
【CateGory Index】: TS255.7
Download(CAJ format) Download(PDF format)
CAJViewer7.0 supports all the CNKI file formats; AdobeReader only supports the PDF format.
【References】
Chinese Journal Full-text Database 8 Hits
1 FU Ruo-nong (Chemistry Department, Beijing Institute of technology, Beijing 100081);Advances and trend of capillary GC chromatographic columns in recent two years[J];Chinese Journal of Analysis Laboratory;2009-03
2 ZHENG Xiang-hua1,HUANG Jia-rong2,WU Ya-ling2 and ZHANG Mao-sheng2(1.Inspection and Quarantine Technical Center,Xiamen Entry-Exit Inspection and Quarantine Bureau,Xiamen 361012;2.Department of Chemistry and Environmental Science,Zhangzhou Normal University,Zhangzhou 363000);Development of new solid-phase microextraction fibers using nano-SiO_2 for the determination of 5 pesticides residues in vegetables[J];Chinese Journal of Analysis Laboratory;2009-08
3 Dan De-zhong,LENG Geng and HUANG Pu-xin(Department of Environmental Science and Engineering,Sichuan University,Chengdu 610065);Analysis of environmental samples[J];Chinese Journal of Analysis Laboratory;2010-07
4 CHEN Liang-bi,MA Chun-hua,ZHAO Jin-yun ( Green chmical engineering key laboratory of Fujian,Department of environmental and architectural engineering,Wuyi University,Wuyishan,Fujian 354300,China);Determination of pyrethrins in tea soups by using solid phase microextraction[J];Journal of Minjiang University;2010-05
5 HUANG Lu1,YANG Min2*,QIAO Ming2,DU Hua-fu2,HUANG Wen-yu2,MENG Jun-hua3.(1.Grade 2006 postgraduate student of College of Pharmacy,Hubei University of Chinese Medicine,Wuhan,430065;2.College of Pharmacy,Hubei University of Chinese Medicine,Wuhan,430065;3.Wuhan No.3 Hospital,Wuhan,430064,Hubei);Determination of organochlorine pesticide residues in Glycyrrhizae and Radix Astragali with Ultrasonic Assisted Extraction and Headspace Solid-phase icroextraction[J];Journal of Hubei University of Chinese Medicine;2009-04
6 Jiang Ruidong(Dandong Center of Quality Inspection and Testing for Agricultural Environment and Products,Dandong 118000,China)Jin Gehui(Huludao Entry-Exit Inspection Quarantine Bureau,Huludao 125000,China);DETERMINATION OF 5 PYRETHROID PESTICIDE RESIDUES IN FRUITS AND VEGETABLES BY GAS CHROMATOGRAPHY[J];Chemical Analysis and Meterage;2009-05
7 CHEN Liangbi MA Chunhua ZHAO Jinyun (he Key Laboratory for Green Chemical lndusty Technology of Fujian Colleges and Universities, Wuyi University, Wuyishan,Fujian 354300);The Research of SPME/GC Technology and Its Application Development[J];Journal of Wuyi University;2009-05
8 DU Xin-zhen,CAO Xu,WANG Xue-mei,CHEN Hui (College of Chemistry and Chemical Engineering,Northwest Normal University,Lanzhou 730070,Gansu,China);Determination of diethyl phthalate by solid-phase microextraction coupled to HPLC using a fiber with mesoporous coating[J];Journal of Northwest Normal University(Natural Science);2009-04
【Citations】
Chinese Journal Full-text Database 4 Hits
1 ZHAO Mingqiao, LI Gongke*, CHEN Hao and ZHANG Zhanxia(School of Chemistry and Chemical Engineering, Sun YatSen University, Guangzhou 510275);Determination of 2,5-cyclohexadiene-1,4-dione,2,6-bis(1,1-dimethylethyl) in seawater by ultrasonic oscillation assisted SPME-GC-MS[J];Analytical Laboratory;2003-06
2 LIU Yong-bo~(*1),ZHAO Hai-feng~2 and ZHANG Ming-xia~1(1.Qingdao Municipal Drainage Monitoring Center,Qingdao 266002;2.Agriculture Bureau of Chengyang District,Qingdao 266109);Determination of Sudan Ⅰ residue by ultrasonic extraction and GC-MS method[J];Chinese Journal of Analysis Laboratory;2006-04
3 HU Ai-jun1,2, LUO Deng-lin1, QIU Tai-qiu1 (1. Light Chemical and Engineering Institute, South China University of Technology, Guangzhou 510640, China; 2. College of Food Engineering and Biotechnology, Tianjin University of Science and Technology, Tianjin 300222, China);Extraction Mechanism of Ultrasound-Enhanced Supercritical Fluids[J];Journal of Chemical Engineering of Chinese Universities;2005-05
4 LU Ping, SONG Bao-An, JIN Lin-Hong, HU De-Yu, HUANG Rong-Mao, YANG Song (Green Pesticide and Bioagricultural Engineering Lab, Education Bureau, Guizhou University, Guiyang 550025; Fine Chemicals Research and Development Center, Guizhou University, Guiyang 550025, China);Determination of Organochlorine Pesticide Residues in Poria cocos by Ultrasonic and Solid Phase Extraction[J];Pesticides;2005-03
【Co-citations】
Chinese Journal Full-text Database 10 Hits
1 WANG Long-geng et al (Agricultural Product Quality Supervision and Inspection Center of Yangzhou,Yangzhou,Jiangsu 225009);Research on the Residues of Pesticides of Organic Phosphorus in the Vegetables[J];Journal of Anhui Agricultural Sciences;2005-05
2 FU Ruo-nong(Department of Chemistry Beijing Institute of Technoligy, Beijing 100081), Fenxi Shiyanshi, 2005, 24(6): 77~92;Advances on gas chromatography in China in recent two years(Ⅲ)[J];Analytical Laboratory;2005-06
3 FU Ruo-nong(Department of Chemistry,Beijing Institute of Technoligy,Beijing 100081);Advances on SPE-chromatography in China in recent two years[J];Chinese Journal of Analysis Laboratory;2007-02
4 CHEN Chen1,2 ZHANG Guo-ping1 ( 1 College of Physical Science and Technology, Central China Normal University, Wuhan 430079, China; 2 School of Physice Seience, Yangtze University, Jingzhou 434023, China );Raman Spectroscopy Technology for Sudan Ⅰ,Ⅱand Ⅲ[J];Optics & Optoelectronic Technology;2007-01
5 LI Hong et al(Department of Chemistry,Hanshan Normal University,Chaozhou,Guangdong 521041);Determination of Sudan Ⅲ in Chili Products by Linear Sweep Polarography[J];Journal of Anhui Agricultural Sciences;2009-36
6 SU De-sheng~1,YU Zhi-gang~2,WANG Shu-jie~3,LI Dong~1,GAO Jiao-yun~1 (1.School of Adult Education,Qingdao University of Science and Technology,Qingdao 266042,China;2.College of Chemistry and Chemical Engineering,Ocean University of China,Qingao 266003,China;3.College of Mechanical and Electrical Engineering,Ocean University of China,Qingao 266071,China);Research on technique and automatic analysis system of harmful algae[J];Marine Environmental Science;2006-02
7 Xu Xiang1,2,Sun Liping1,2,*Dong Jie1,2(1.Institute of Bee Research,Chinese Academy of Agricultural Sciences,Beijing100093,China;2.National Research Center of Bee Product Processing,Ministry of Agriculture,Beijing100093,China);Effects of Ultrasound Enhancement on the Constituents of Propolis Oleoresin Extracted by Supercritical CO_2[J];Academic Periodical of Farm Products Processing;2008-11
8 XU Yun-cheng1, ZHAO Yun-he2, ZHU Jie-li1, ZHANG Yu1, FAN Zhi-xian1(1.Jilin Agricultural University, Changchun 130118, Jilin, China; 2. Shenyang Agriculture University, Shenyang 110161, Liaoning, China);Dynamics of linuron residues in corn and soil[J];Agrochemicals;2006-02
9 TAN Wei,QIU Tai-qiu(College of Light Industry and Food Sci.,South China Univ.of Technol., Guangzhou 510640,China);Effect of Ultrasonic Field on Extracting Oil From Sunflower Seed Using Sub-critical Carbon Dioxide[J];Journal of Sichuan University(Engineering Science Edition);2007-03
10 PAN Zhiming LI Zhong WANG Bing ZHOU Luming(Deyang Product Quality Supervision and Inspection Institute,Deyang 618000);Progress on Determination of Sudan Dyes in Foodstuffs[J];World Sci-Tech R & D;2007-06
China Proceedings of conference Full-text Database 1 Hits
1 MI Jianping;DEVELOPMENT OF DETERMINATION OF SUDAN COLORANTS IN FOODS[A];[C];2008
【Secondary References】
Chinese Journal Full-text Database 3 Hits
1 ZHANG Mao-sheng1,HUANG Jia-rong2,ZHENG Xiang-hua3 and CHEN Hui-ling1 (1.Department of Chemistry and Environmental Science,Zhangzhou Normal University,Zhangzhou 363000;2.Zhangzhou Entry-Exit Inspection and Quarantine Bureau,Zhangzhou 363000;3.Inspection and Quarantine Technical Center,Xiamen Entry-Exit Inspection and Quarantine Bureau,Xiamen 361012);Determination of benzene,toluene and xylenes in waters by gas chromatography with dispersive liquid-liquid microextraction[J];Chinese Journal of Analysis Laboratory;2010-06
2 Dan De-zhong,LENG Geng and HUANG Pu-xin(Department of Environmental Science and Engineering,Sichuan University,Chengdu 610065);Analysis of environmental samples[J];Chinese Journal of Analysis Laboratory;2010-07
3 ZHANG Mao-sheng 1,HUANG Jia-rong 2,ZHENG Xiang-hua 3,WU Ting 1(1.Department of Chemistry and Environmental Science,Zhangzhou Normal University,Fujian 363000,China;2. Zhangzhou Entry-Exit Inspection and Quarantine Bureau,Fujian 363000,China;3.Inspection and Quarantine Technical Center,Xiamen Entry-Exit Inspection and Quarantine Bureau,Xiamen 361012,China);Stainless Steel Wire Supported SiO_2/poly(dimethylsiloxane) Encapsulating Multi-wall Carbon Nanotubes Complex Membrane Solid Phase Microextraction for Analyzing Trace Benzene,Toluene,Xylene in Water Samples[J];Journal of Zhangzhou Normal University(Natural Science);2010-04
【Secondary Citations】
Chinese Journal Full-text Database 10 Hits
1 QIU Tai-qiu1, YANG Ri-fu1, HU Ai-jun1, YAN Jie1, LIANG Han-Hua2 (1.College of Food and Biological Engineering, South China University of Technology,Guangzhou 510640,China; 2.Department of Applied Biological and Chemical Technology, Homgkong Polytechnic University, Hongkong);Influencing Factors in Ultrasonic Enhanced Supercritical Fluid Extraction for Extrating CLSO and CLSE from Coix Lacryma-jobi Seeds[J];Journal of Chemical Engineering of Chinese Universities;2005-01
2 Wang Qiang(Chemistry Depaltment, Huazhong University of Science and Technology)Long Yaoting Lu miaoqin Wang Zijian(Research Center for Eco-Environmental Science, Academia Sinica)He Rungen Wang Dahui(Research Institute of Biophysics, Academia Sinica);IDENTIFICATION OF FREE RADICALS AND SOME ORGANIC COMPOUNDS IN THE DRINKING WATER FROM KASHIN-BECK DISEASE REGION OF FENGNING COUNTY[J];Environmental Chemistry;1989-02
3 Wang Yizhong Chen Qagxin Hu Keyan(Research Center for Eco-Environmental Sciences, Chinese Academy of Sciences, Beijing, 100085);STUDY ON DESTRACTION OF BENZENE RING STRUCTURE BY PHOSPHORUS OXYGEN REACTION[J];Environmental Chemistry;1995-01
4 Wang Yizhong Liu Jiang Hu Chun Tang Hongxiao(Research Center for Eco-Environmental Sciences. Chinese Academy of Sciences. Beijing. 100085);ANALYSIS OF ORGANIC CONTAMINANTS IN THE WATER OF BAI-YANG-DIAN LAKE[J];Environmental Chemistry;1995-05
5 YANG Li-li,DENG Yan-hui (Nanjing Environmental Monitoring Center, Nanjing, Jiangsu 210013,China);Detection of Residual BHC and DDT in Soil Using Ultrasonic Extraction -GC[J];The Administration and Technique of Environmental Monitoring;2002-03
6 WANG Mei, ZHANG Xin-min (Taizhou Environmental Monitoring Center, Taizhou, Jiangsu 225300, China);Development of Environmental Organic Pollutants' Analysis Method and Trace Enrichment Technology in China[J];The Administration and Technique of Environmental Monitoring;2004-01
7 LANG Yinhai~(1,2), JIANG Xin~(1*), ZHAO Zhenhua~1, ZHAO Qiguo~1 (1.Institute of Soil Science, Chinese Academy of Sciences, Nanjing 210008;2.College of Environmental Science and Engineering, Ocean University of China, Qingdao 266003);Studies on the ultrasonic extraction and GC determination of 13 organochlorine pesticides in two soils[J];Acta Scientiae Circumstantiae;2004-02
8 Gao Hong, Jin Lingren, Li Hongli(Shandong Province Environmental Monitoring Center, Jinan 250013, China);EXTRACTION AND ENRICHMENT TECHNIQUES IN SAMPLE ANALYSIS BY GAS CHROMATOGRAPHY[J];Chemical Analysis and Meterage;2004-02
9 XU Xing-yi,LIU Jin-song,PANG Xiao-lu (Zhejiang Province Environmental Monitoring Centre, Hangzhou 310012,China);The research of pre-treatment method for detection of Pesticide residue in soil[J];Environmental Monitoring In China;2004-01
10 WANG Su-Juan 1,PEI Yue-Hu 1,SUN Xiu-Yan 2 ( 1 School of Traditional Chinese Material Medica,Shenyang Pharmaceutical University,Shenyang 110016,China; 2 Center of Instrument Analysis,Shenyang Pharmaceutical University,Shenyang 110016,China);EI,NCI and PCI Mass Spectrum of Organochloride and Organophosphorous Pesticides[J];Pesticides;2004-08
©2006 Tsinghua Tongfang Knowledge Network Technology Co., Ltd.(Beijing)(TTKN) All rights reserved