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《Chinese Journal of Analysis Laboratory》 2014-08
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Determination of four nitrofuran antibiotics in anti-acne cosmetics by HPLC and their verification by HPLC-MS /MS

MENG Xiansshuang;MA Qiang;ZHANG Qing;LI Jing-rui;CHEN Yun-xia;WANG Yuan-cheng;MA Hui-juan;L Qing;BAI Hua;Chinese Academy of Inspection and Quarantine;  
An assay was established for the simultaneous determination of four nitrofurans(furadantin,furazolidone,furaltadone and furacilin) in acne cosmetics using high performance liquid chromatography(HPLC) and their verification by HPLC-MS/MS.Samples were ultrasonically extracted by acetonitrile +methanol(70 + 30,V /V) and filtered by microporous membrane filter.The separation of analytes was achieved by an XTerra MS C18(4.6 mm ×250 mm,5 μm) column using 15 mmol/L ammonium acetate and acetonitrile in gradient elution.Quantification was carried out by external standard method and the suspected positive samples were verified by HPLC-MS /MS method.Results indicated that four nitrofurans showed good linearities and the limits of quantification(LOQs) of furadantin,furazolidone,furaltadone and furacilin were 5,5,7.5,5 mg /kg,respectively.Average recoveries of four target compounds ranged from 85.0% to 99.6% at three spiked levels with relative standard deviations between 2.1% and 9.5%.
【Fund】: 质检公益性行业科研专项(2012104013-4);; 国家科技支撑计划项目(2013BAK04B03)资助
【CateGory Index】: O657.63;TQ658
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【Citations】
Chinese Journal Full-text Database 8 Hits
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【Co-citations】
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