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《Journal of Molecular Catalysis》 2004-01
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Preparation and Characterization of ZnAlCe-hydrotalcitelike Compounds[ZnAlCe-HTLcs]

XIE Xian-mei, AN Xia, LI Jin-ping, WANG Xiu-lan, WANG Zhi-zhong(Taiyuan University of Technology, Taiyuan 030024, China)  
The preparation of ZnAlCe-Hydrotalcite Like-Compounds[ZnAlCe-HTLcs] was studied. ZnAlCe-HTLcs were synthesized by a method of variable pH with the materials of Zn(N_3)\-2、 Ce(N_3)\-3、 Al(N_3)\-3 and NaOH. The evolution of versus NaOH(mmol) during the basic titration of solutions containing M~(2+)/M~(3+)=2.0, Ce~(3+)/Al~(3+)=0.25 was studied. Phases of synthesized compounds at different pH were detected by XRD.It was shown that the pure ZnAlCe-HTLcs can be prepared at M~(2+)/M~(3+)=2, Ce~(3+)/Al~(3+)=0.07~0.50 pH=5.8~6.5. The properties of ZnAlCe-HTLcs were characterized by XRD, FT-IR and ICP. The composite oxides derived from ZnAlCe-HTLcs have been used in the catalytic reduction of NO . The experimental results show that the conversion of NO is up to 100% at 680 ℃.
【Fund】: 山西省自然科学基金资助项目(20001015).
【CateGory Index】: O643.3
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