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《Journal of Molecular Catalysis》 2005-03
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Photocatalytic Activity of TiO_2 Prepared by Ultrasonic Hydrolytic Methods

WU Shu-xin~(1, 2, 3), YIN Yan-hua~2, MA Zhi~1, QIN Yong-ning~(*1), QI Xiao-zhou~1, LIANG Zhen-cheng~1(1. School of Chemical Engineering and Technology, Tianjin university, Tianjin 300072, China; 2. The 718th Research Institute, Handan, 056027, China; 3. Institute of Advanced Catalysis and Technology, Tangshan Teachers College, Tangshan, 063000, China)  
Nanosized anatase TiO_2 has been widely used in the field of environmental protection because of its excellent performance in photocatalysis. In this paper, anatase TiO_2 with particle size ranging from 5 nm to 6 nm were abtained at room temperature by the hydrolysis of TiCl_4 under the irradiation of ultrasonication. The effect of ultrasonication, calcinations temperature and particle size on the photocatalytic activity was investigated. The results show that inflicting the ultrasonic irradation upon the preparing process markedly affects the catalyst, i.e., the degradation rate of formic acid are raised from 68.57% to 97.13% and this excellent performance can be found among a wide range of calcinations temperature. With the decrement of particle size, the photocatalytic activity increases, and the quantum size effect was found when the size of TiO_2 was less than 20 nm.
【Fund】: 南开大学-天津大学联合研究院教育部重点基金资助项目.
【CateGory Index】: O643.361
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