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《Journal of Molecular Catalysis》 2007-03
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Photocatalytic Properties of B-doped Cd_(0.5)Zn_(0.5)S Photocatalyst for Hydrogen Generation

ZHUGE Fu-yu1,2,JIN Zhi-liang1,LV Gong-xuan1*(1.State Key Laboratory for Oxo Synthesis and Selective Oxidation,Lanzhou Institute of Chemical Physics,The Chinese Academy of Sciences,Lanzhou 730000,China;2.Graduate school of the Chinese academy of Sciences,Beijing 100101,China)  
In this paper,a novel photocatalyst,B/Cd0.5Zn0.5S,was prepared by impregnation of H3BO3 coupled with catalyst Cd0.5Zn0.5S.Photocatalytic activity and stability for hydrogen production of B/Cd0.5Zn0.5S under visible light irradiation have been studied.It was found that Cd0.5Zn0.5S catalyst doped with 2% boron showed a maximum rate of hydrogen evolution.The activity of hydrogen evolution from aqueous sodium sulfite solution under visible light irradiation and long-term stability were improved.The catalysts were characterized using XRD、 XPS﹑PL、 UV-Vis techniques and the possible reaction mechanism was discussed.The diffuse reflectance and photoluminence spectral intensity of the B-doped Cd0.5Zn0.5S were enhanced greatly.B species did not exist in the form of oxide in the catalyst.There was interaction between B and Cd0.5Zn0.5S catalyst,which improved photocatalytic properties.
【Fund】: 973资助项目(No.G200000264)
【CateGory Index】: O643.32;TQ116.2
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