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《JOURNAL OF MOLECULAR CATALYSIS (CHINA)》 1996-02
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Preparation and Physicochemical Characterization of Novel Catalyst Material Mg-Al Complex Oxides

Yang Xiyao;Ren Shaoling;He Hui;Wang Daqing(Catalysis Section,College of Chemistry and Molecular Engineering,Peking University,Beijing 100871)  
Magnesium aluminum hydrotalcites with the molar ratios of MS to Al of 3-6.7 were perpared by coprecipitating an aqueous solution of magnesium and aluminum salts with NaOH-Na2CO3 or NH4OH-(NH4) 2CO3 mix solution.By calcinating the hydrotalcites at 500-600℃ the Mg-Al complex oxides,Mg(Al) O were produced.XRD determination confirmed that Mg(Al) O has the same crystal structure as MgO.The B E T determination showed most of the Mg(Al) O have large surface area(180-235m2/g) and high thermal stability.The basic characters of Mg(Al) O were investigated by CO2 adsorption,CO2-TPD and isoelectric point determinations.It was found that the basic center density and basic center distribution of Mg(Al) O are similar to those of MgO.On the other hand,it was confirmed by NH3-TPD determination that,Mg(Al) O retained some acidity properties like those of γ-Al2O3.
【Fund】: 中国石油化工总公司顾问委员会基础研究基金
【CateGory Index】: O611
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