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《Guangdong Chemical Industry》 2011-04
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Teaching Experiment Design of N-butyl Acetate Green Synthesis

Huang Guowen,Gao Huanfang,Chen Zhi,Xu Junqiang,Li Jun,Quan Xuejun(College of Chemistry and Chemical Engineering,Chongqing university of Technology,Chongqing 400054,China)  
Environment-friendly sulphonated carbon materials were made from starch,and the n-butyl acetate were synthesized with sulphonated carbon materials and sulfuric acid.In comparison with the traditional process routes of n-butyl acetate that synthesized with sulfuric acid,the result showed that solid acid catalytic process routes had easily controled reaction conditions,safe and reliable,less by-products,simple post-treatment process,less waste water,catalyst easy to be recycled and reused.Based on the optimization experiment process,an organic synthesis experimental teaching programme had been designed out.Because of the esterification conversion calculated on the basis of collected water,the experimental process had been simplified.Teaching practices showed that students'learning enthusiasm and initiatives were aroused.The experiment design can be used in undergraduate organic synthesis experiment,green process design and kinetic teaching experiment.It will help to establish the environment-friendly chemical engineering laboratory.
【Fund】: 重庆理工大学高教研究项目(20100035);重庆理工大学实验技术开发基金(32-03)
【CateGory Index】: TQ225.241-4
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