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《Chemical Research In Chinese Universities》 1989-12
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Studies on Voltammetric Adsorptive Wave of Gallium-Salicyl Fluorone Complex

Chen Rongli, Zhang Xiaoli, Wang Lizeng, Wang Shuren (College of Chemistry, Shandong University, Jinan)  
In a supporting solution containing 5. 0× 10 6 mol/L salicyl fluorone, 0. 2 mol/L potassium hydrogen phthalate- HCl , at pH = 3. 0, a sensitive adsorptive wave of gallium- salicyl fluorone complex was obtained by using linear scanning voltammetry. The peak potential is - 0. 93 V(vs, SCE). The change of peak height with the concentration of gallium is linear in the range of 7. 5× 10-9-3. 8× 10-7 mol/L. The electrode processes of the adsorptive wave of the complex may be presented as follows :1. Complexing reaction in the bulk solution is2.GaH3L2+ diffuses to the electrode surface and is adsorbed on it3. When Ep( 2) = - 0. 93 V, the ligand and the center ion of the complex are simultaneously reduced
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