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《Chemical Research In Chinese Universities》 1990-03
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An Electrochemical Study on Binuclear Big Bird Complexes of Ni( Ⅱ ) and Cu( Ⅱ )

Luo Qinhui, Yang Sheng, Shen Mengctutng, Peng Qingyun (Coordination Chemistry Research Institute, Nanjing University, Nanjing)  
We studied by cyclic voltammetry the oxidation-reduction process of binuclear Big Bird complexes of Ni( Ⅱ ) and Cu( Ⅱ ). Big Bird ligand was synthesized by condensation of tert-buty 1-2,6-diformyl-phenol with 4-n- hexyl- thiourea. The interaction between two central atoms in binuclear complexes and their rate constants of electrode reaction were also investigated. Activation of CO by Ni( Ⅱ ) complex was verified by IR and cyclic voltammetry.
【Fund】: 国家自然科学基金
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