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《Chemical Research In Chinese Universities》 1990-12
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A New Steroidal Saponin from Smilax Menispermoides

Ju Yong, Jia Zhong-jian (Institute of Organic Chemistry, Lanzhou University, Lanzhou 730000)  
A new steroidal saponin, m. p. 310℃, [a]20D= -90. 0℃, was isolated from 70% alcoholic crude saponin extract of the rhizome of Smilax menispermoides D. C. by silica gel column chromatogra-phy and further purified by Sephadex LH-20. Its structure was determined as : (25D) spirost-5-en-3β, 17α,27-triol-3-O-[β-L-rhamnopyranosyl (1-2)] [a-L-rhamnopyranosyl (1-4)]-α-D-glucopyra-noside by means of IR, MS, 13C NMR, DEPT and chemical methods.
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