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《Chemical Research In Chinese Universities》 1991-12
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A Simple UV-Visible, Circular Dichroism Thin-layer Spectroelectro- chemical Cell with Long Optical Path

Zhu Yong-chun (Shenyang Medical College, Shengyang, 110031)Cheng Guang-jin, Dong Shao-jun (Changchun Institute of Applied Chemistry,Chinese Academy of Sciences,Changchun, 130022)  
A simple UV-visible, circular dichroism thin-layer spectroelectrochemical cell with long optical path has been designed and characterized. The cell with 10 mm quartz cuvette as the optical window, two pieces of 5 mm×10 mm×15 mm teflon as the electrode supporters and a glassy carbon slide as the working electrode has an adjustable thickness of thin-layer. We have carried out the optical and electrochemical experiments of characterization with K3Fe(CN)s and tyrosine working system, which show the cell has a very good thin-layer electrochemistry character and fast spectroelectrochemistry response. The cell can also be used in circular dichroism electrochemistry study.
【Fund】: 国家自然科学基金
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