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《Chemical Research In Chinese Universities》 1992-03
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Studies on Fluorimetric Reaction of Salicyl aldehyde Isonicotinylhydrazone with Gallium

CUI Wan-cang, TANG Bo, SHI Hui-ming (Department of Chemistry, Nankai University, Tianjin, 300071)  
The fluorimetric reaction of salicylaldehyde isonicotinylhydrazone with gallium has been studied. The constants for dissociation of the reagent were established. The fluorescence excitation and emission wavelengths of the complex of gallium with the reagent are 395 nm and 480 nm, respectively. The sensitivity of the method is 4. 0×10-4 ppm. The linear range is 0-1.0 μg/10 mL. The molar ratio of gallium to reagent was found to be 1 : 1. The proposed mathod has been used for the determination of trace gallium in geologic samples with satisfactory results.
【Fund】: 国家自然科学基金
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