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《Chemical Research In Chinese Universities》 1993-03
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Synthesis of α- and β-Cs_4H_3[SiW_3O_(37)Cr_3(H_2O)_3] · xH_2O and Their Catalysis of Epoxidation of Olefin by PhIO

LIU Jing-Fu , ZHAO Ben-Liang, LI Jin-Chang, XU Gui-Ying, ZHU Zhi-Ping (Department of Chemistry, Northeast Normal University, Changchun, 130024)  
The synthesis of α- and β-CsH3[SiW9O37Cr3(H2O)3] β xH2O and their catalysis for epoxi-dation of olefin are reported. The heteropolyacid salts have an ability to catalyze the epoxidation of olefin by PhIO, and the catalytic activity of them is probably related to the fact that the substituted Cr ( Ⅲ ) can be oxidized to a higher oxidation state and the compound with a higher oxidation state has an oxidation property.
【Fund】: 国家自然科学基金
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