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《CHEMICAL RESEARCH IN CHINESE UNIVERSITIES》 1997-09
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Studies on Application of Microwave Heating Techniques for the Solid State Reactions of Coordination Compounds(Ⅰ)── Synthesis of Co(Ⅱ), Ni(Ⅱ), Cu(Ⅱ) Complexes by Solid State Reactions Under Microwave

JIA Dian-Zeng; YANG Li-Xin; XIA Xi(Department of Chemistry, Xinjiang University, Urumqi, 830046)XIN Xin-Quan(Institute of Coordination Chemistry, Nanjing University, Nanjing, 210093)  
Solid state reactions of the transition metal acetates such as Co (OAc)2·4H2O,Ni(OAc)2·4H2O,Cu (OAc)2·H2O with organic compounds such as amino acids, Schiffbases, β-diketon, 8-hydroxyquinoline have been investigated in the microwave oven. It isshown that the coordination compounds can be synthesized by solid state reactions up to 50times faster in a microwave oven than by conventional techniques. The results suggest asignificant Potential value of microwave heating in solid state coordination chemistry.
【Fund】: 国家自然科学基金
【CateGory Index】: O614
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