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《Chemical Research In Chinese Universities》 2001-06
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Synthesis and Characterization of Novel Functional Hyperbranched Polyesters

TANG Li Ming (Dept. of Chem. Eng., School of Material Science and Engineering, Tsinghua University, Beijing 100084, China) Hans R. Kricheldorf (Institute of Technology and Macromolecule Chemistry, Hamburg University, Hamburg, Germany)  
A series of hyperbranched polyesters with controlled inherent viscosities have been prepared by polycondensation of 3,5 bis(trimethylsiloxy) benzoyl chloride with sililated p methyl aniline under various molar ratios. After reacted with acid chlorides in o dichlorobenzene, the functionalization of these polyesters was readily accomplished. The end groups of the crude polymers were effectively transferred into vinylic and ethynylic groups in high yields(85%) as calculated by 1H NMR spectra without any change in their inherent viscosities.
【CateGory Index】: O631
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