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《Chemical Research In Chinese Universities》 2002-05
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Identification of the Flavonoid Constituents from Leaves of Acanthopanax Senticosus Harms

CHEN Mao-Lian, SONG Feng-Rui, GUO Ming-Quan, LIU Zhi-Qiang, LIU Shu-Ying* (Changchun Institute of Applied Chemistry, Chinese Academy of Sciences, Changchun 130022. China)  
Abstract Four flavonoids from leaves of Acanthopanax Senticosus Harms were observed in negative ion mode in the electrospray mass spectra. Two of them were further isolated and identified as quercitrin (quercetin-3-O- -L-rhamnoside) and hyperin (quercetin-3-O- -D-galactoside) on the basis of MSn and NMR data. The other two compounds in the mixtures were tentatively established as quercetin and rutin ( quercetin-3-O-rutinoside) in terms of their electrospray tandem mass spectrometry (ESI-MSn) data. Three of the four flavonoids (excluding hyperin) haven't been reported in this plant before.
【Fund】: 吉林省科技厅重点发展项目(批准号:1999·0310-2)资助.
【CateGory Index】: O629
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【References】
Chinese Journal Full-text Database 10 Hits
1 Liu Gui-ping~1,Li Zhi~2 (1 Harbin Pharmaceutical Group Sixth Pharm Factory,Harbin 150056,China; 2 Harbin Pharmaceutical prepared slices of Chinese crude drugs limited liability company,Haerbin 150088,China);Isolation and Identification of Chemical Constituents of Flavones from the Fruits of Acanthopanax Senticosus Harms[J];Chinese Journal of Medicinal Guide;2011-02
2 ZHU Jing-bo1,LI Dan-feng1,QIU Huan-jie1,WANG Long-xing2,XIAO Hong-bin21.School of Biological & Food Engineering,Dalian Polytechnic University,Dalian 116034,China;2.Dalian Institute of Chemical Physics,Chinese Academy Sciences,Dalian 116023,China;HPLC/ESI-MS analysis of flavonoids in Epimedium extract[J];Journal of Dalian Polytechnic University;2009-05
3 Dou Jianpeng, Liu Zhiqiang, Liu Shuying * (Laboratory of New Drug Research, Changchun Institute of Applied Chemistry, Chinese Academy of Sciences, Changchun 130022);Studies on Anhydroicaritin by Electrospray Ionization Multi-stage Tandem Mass Spectrometry[J];Chinese Journal of Analytical Chemistry;2003-12
4 GUO Ming-Quan, SONG Feng-Rui, CHEN Mao-Lian, BAI Yu, LIU Zhi-Qiang , LIU Shu-Ying (Changchun Institute of Applied Chemistry, Chinese Academy of Sciences, Changchun 130022, China);Studies on Oligosaccharides from Acanthopanax Senticosus Harms (AS) by Electrospray Ionization Tandem Mass Spectrometry(MS~n)[J];Chemical Research In Chinese Universities;2003-09
5 SUN Ping, LUO Guo-An *, QU Jun (Department of Chemistry, Tsinghua University, Beijing 100084, China);Research on the Stability of Relative Strength of Sub-ion in ESI-MS-MS Analysis[J];Chemical Research In Chinese Universities;2003-12
6 LIU Chun-Ming 1,2, LIU Zhi-Qiang 1*, DOU Jian-Peng 1, LI Li 1, LIU Shu-Ying 1* (1. Laboratory of New Drug Research, Changchun Institute of Applied Chemistry, Chinese Academy of Sciences, Changchun 130022, China; 2. Department of Chemistry, Changchun Teachers College, Changchun 130022, China);Isolation and Structure Identification of the Novel Alkaloid Constituent from Epimedium Koreanum Naki[J];Chemical Research In Chinese Universities;2003-12
7 WANG Yong 1,2, SONG Feng-Rui1, JIN Dong-Ming1, LIU Zhi-Qiang 1*, LIU Shu-Ying 1* (1. The New Drug Lab of Changchun Institute of Applied Chemistry, Chinese Academy of Sciences, Changchun 130022, China; 2. Faculty of Chemistry, Northeast Normal University, Changchun 130024, China);Studies on the Aconitum Alkaloids in the Sini Concoction by Electrospray Ionization Mass Spectrometry[J];Chemical Research In Chinese Universities;2004-01
8 HUANG Lan-Fang 1, LIANG Yi-Zeng 1 *, GUO Fang-Qiu 1, CHEN Ben-Mei 2 (1. College of Chemistry and Chemical Engineering, Central South University, Changsha 410083, China; 2. Analytical Testing Center of Xiangya Medical College, Central South University, Changsha 410078, China);Simultaneous Separation and Determination of Arginine and Methylated Arginines in Human Plasma with LC-APCI-MS Method[J];Chemical Research In Chinese Universities;2004-02
9 BAI Yu, GUO Ming-Quan, SONG Feng-Rui, LIU Zhi-Qiang *, LIU Shu-Ying * (Changchun Institute of Applied Chemistry, Chinese Academy of Sciences, Changchun 130022, China);Studies on Flavonoids from Sophora Flavescens Ait Using ESI-MS~n[J];Chemical Research In Chinese Universities;2004-02
10 DOU Jian-Peng, LIU Zhi-Qiang *, LIU Shu-Ying *(Laboratory of New Drug Research, Changchun Institute of Applied Chemistry, Chinese Academy of Sciences, Changchun 130022, China);Studies on Icariin by Electrospray Ionization Mass Spectrometry[J];Chemical Research In Chinese Universities;2004-05
China Proceedings of conference Full-text Database 1 Hits
1 DOU Jian-peng, LIU Zhi-qiang, LIU Shu-ying(Laboratory of New Drug Research, Changchun Institute of Applied Chemistry, Chinese Academy of Sciences, Changchun 130022, China);Studies on Flavonoids Extracted From Epimedii Herba by Electrospray Ionization Multi-stage Tandem Mass Spectrometry[A];[C];2003
【Citations】
Chinese Journal Full-text Database 2 Hits
1 GU Jing-Kai, ZHONG Da-Fang, CHEN Xiao-Yan, ZHOU Hui, SHEN Jia-Cong ( College of Life Science, Key Lab. for Supramolecular Structure and Spectroscopy, Jilin University, Changchun 130023, China; Lab. of Drug Metabolism and Pharmacokinetics, Shengyang Pharmaceutical University, Shenyang 1 10015, China) LIN Yang (PLA Dalian Junior College of Medicine, Dalian 116017, China);Identification of Major Metabolites of Etofesalamide in Rabbits by Liquid Chromatography/Ion Trap Mass Spectrometry[J];Chemical Research In Chinese Universities;2000-05
2 CUI Meng, LIU Zhi Qiang, SONG Feng Rui, LIU Shu Ying * (Changchun Institute of Applied Chemistry, Chinese Academy of Sciences, Changchun 130022, China);Studies on Negative Electrospray Ionization Mass Spectrometry on Saponins[J];Chemical Research In Chinese Universities;2001-08
【Co-citations】
Chinese Journal Full-text Database 10 Hits
1 Bai Yu, Chen Maolian, Song Fengrui, Xing Junpeng, Liu Zhiqiang *, Liu Shuying * (Changchun Institute of Applied Chemistry, New Drug Laboratory, Chinese Academy of Sciences, Changchun 130022);Multi-Tandem Mass Spectrometric Analysis of Rutin-Copper (Ⅱ) Complex[J];Chinese Journal of Analytical Chemistry;2004-09
2 CUI Yan~(1),ZHANG Xiu-feng~(2),LIU Yang~(2),YAN Bao-zhen~(*1) (1.Faculty of Science,Beijing University of Chemistry Technology,Beijing 100029;2.State Key Laboratory for Structural Chemistry of Unstable and Stable Species,Center for Molecular science,Institute of Chemistry,Chinese Academy of Sciences,Beijing 100080);Study on Diosgenin Glycosides from Paris polyphylla Smith by High Performance Liquid Chromatography-Tandem Mass Spectrometry[J];Journal of Analytical Science;2006-05
3 GU Jing Kai 1 * , CHU Da Feng 1, ZHONG Da Fang 1,4 , LI Yan 2 ZHOU Hui 1, SHEN Jia Cong 3 (1. College of Life Science, 2. College of Chemistry, 3. Key Lab. for Supermolecular Structure and Spectroscopy, Jilin University, Changchun 130;Studies on the Electrospray Ion Trap Mass Spectra of SFZ-47 and Its Metabolites for a Novel Anti-inflammatory and Analgesic Agent[J];Chemical Research In Chinese Universities;2002-02
4 CHU Da\|Feng\+1, GU Jing\|Kai\+\{1 *\}, ZHONG Da\|Fang\+\{1,2\}, SI Duan\|Yun\+2, ZHOU Hui\+1 (1. College of Life Science, Jilin University, Changchun 130023, China; 2. Lab of Drug Metabolism and Pharmacokinetics, Shenyang Pharmaceutical University,;Isolation and Identification of Etofesalamide-2-glucuronide[J];Chemical Research In Chinese Universities;2002-03
5 DOU Jian-Peng, LIU Zhi-Qiang *, LIU Shu-Ying *(Laboratory of New Drug Research, Changchun Institute of Applied Chemistry, Chinese Academy of Sciences, Changchun 130022, China);Studies on Icariin by Electrospray Ionization Mass Spectrometry[J];Chemical Research In Chinese Universities;2004-05
6 WU Wei, SONG Feng-Rui, LIU Zhi-Qiang, LIU Shu-Ying* (Laboratory of New Drug Research, Changchun Institute of Applied Chemistry, Chinese Academy of Sciences, Changchun 130022, China);Differentiation of the Flavonoid C-glycoside Isomers in Scutellaria baicalensis Georgi Using HPLC-ESI-MS/MS[J];Chemical Research In Chinese Universities;2005-01
7 DAI Yulin;YU Shanshan;ZHANG Ying;HAO Ying;ZHONG Wei;YUE Hao;LIU Shuying;Jilin Ginseng Academy,Changchun University of Chinese Medicine;Changchun Institute of Applied Chemistry,Chinese Academy of Sciences;;Studies on the Isoflavone in Extract of the Flower of Pueraria Lobata by RRLC-Q-TOF MS/MS[J];Chemical Journal of Chinese Universities;2014-07
8 XU Yuan-jin~(1,2),LI Yong-ku~1 (1.Engineering Center for Sugar Cane and Cane Sugar,Guangxi University,Nanning 530004,China;2.Guangxi Key Laboratory of Subtropical Bioresource Conservation and Utilization,Guangxi University,Nanning 530004,China);Analysis of Seven Organophosphorous Pesticides in Vegetables by Liquid Chromatography-Electrospray Ion Mass Spectrometry[J];Journal of Instrumental Analysis;2006-04
9 YANG Wei-cheng;LV Jing;QI Qing-rui;SHENG Li-yan;LI Mei-hua;YANG Chao;LUO Yong;R & D Center,Shanghai Research Institute of Chemical Industry;Branch of Professional Education,Xinjiang Education Institute;;Synthesis of Isotope labeled Trichlorfon-methoxyl-D_6 and Dichlorophos-methoxyl-D_6[J];Journal of Isotopes;2014-01
10 ZHANG Lei 1, WANG Zhi cai 1, GUO Ming quan 2, CHEN Yan ping 1, MA Xing yuan 1 (1 College of Chemistry, Jilin University, Changchun 130021, China; 2 Changchun Institute of Applied Chemistry, Chinese Academy of Sciences, Changchun 130022, China);Identification of three saponins from leaves of Aralias elate[J];Chinese Traditional and Herbal Drugs;2004-09
China Proceedings of conference Full-text Database 1 Hits
1 SUN Yu-Ming~1, MA Gui-Lei~2, HUANG Hai-Hua~2, ZHONG Da-Fang~1(1. Laboratory of Drug Metabolism and Pharmacokinetics, Shenyang Pharmaceutical University, Shenyang 110016, China; 2. Department of Pharmaceutical Microbiology, Shengyang Pharmaceutical University, Shenyang 110016, China);Identification of the Metabolites of Etofesalamide by Microbial Transformation With LC-MS~n[A];[C];2003
【Co-references】
Chinese Journal Full-text Database 10 Hits
1 WANG Xin,HAI Chun-xu,LIANG Xin(Department of Toxicology,School of Military Preventive Medicine,the Fourth Military Medical University,Xi'an 710032,China);Activities of Acanthopanax Extracts in Vitro in Free Radical Models[J];Carcinogenesis,Teratogenesis & Mutagenesis;2009-02
2 GUO Xue-feng et al (International Centre for Bamboo and Rattan, SFA Key Open Laboratory on Bamboo and Rattan Science and Technology, Beijing 100102);Research Advances in Extraction, Isolation, Purification and Content Determination of Methods Flavonoids[J];Journal of Anhui Agricultural Sciences;2007-26
3 DAI Yu-jun et al (College of Life Science and Technology,Xiaogan University,Xiaogan,Hubei 432000);Study on Extracting Total Flavone with Water from the Leaves of Ginkgo biloba L.[J];Journal of Anhui Agricultural Sciences;2008-01
4 CAI Zheng-wang et al (Department of Chemistry and Life Science,Ankang University,Ankang,Shaanxi 725000);Research Advance on Clematis Plants[J];Journal of Anhui Agricultural Sciences;2008-18
5 ZHAO Yong-guang et al(Hebei Normal College of Science & Technology,Changli,Hebei 066600);Study on Application of Total Flavonoids Extraction from Platycladus orientalis Leaf in Functional Shampoo[J];Journal of Anhui Agricultural Sciences;2008-24
6 XIONG Ya-nan et al(Biological Science Department of North China Coal Medical College,Tangshan,Hebei 063000);Study on Isolation and Distribution of Endophytic Fungus in Eleutherococcus senticosus Harms[J];Journal of Anhui Agricultural Sciences;2009-24
7 XING Zhao-bin et al (Department of Biology,North China Coal Medical College,Tangshan,Hebei 063000);Effects of Endophytic Fungi on the Content of Eleutherosides B and E in Eleutherococcus Senticosus[J];Journal of Anhui Agricultural Sciences;2009-25
8 QING Yi-wei et al(Department of Chemistry,Qinghai Normal University,Xining,Qinghai 810008);Study on the Polysaccharide Contents of Dracocephalum tanguticum Maxim by Different Extract Methods[J];Journal of Anhui Agricultural Sciences;2009-26
9 ZHOU Li-bing et al (Qianxinan Vocational and Technical College for Nationalities,Xingyi,Guizhou 562400);Principal Component Analysis and Cluster Analysis of Trace Elements in Plant Nitraria Leaf from Qinghai Region[J];Journal of Anhui Agricultural Sciences;2010-13
10 WANG Ling et al(School of Physics and Chemistry,Xihua University,Chengdu,Sichuan 610039);Extraction of Pomegranate Peel Polyphenols and Its Antimicrobia Activities[J];Journal of Anhui Agricultural Sciences;2010-17
【Secondary References】
Chinese Journal Full-text Database 10 Hits
1 HAN Zhong-ming et al(College of Chinese Medicinal Materials,Jilin Agricultural University,Changchun,Jilin 130118);Study on the Module Biomass Forecast of Acanthopanax senticosus Population[J];Journal of Anhui Agricultural Sciences;2008-30
2 LI Ya-jing et al (Zhejiang Economic and Trade Polytechnic,Hangzhou,Zhejiang 310018);Effect of Complex Liquid of Gynostemma pentaphllum on Fatigue Resistance of Mice[J];Journal of Anhui Agricultural Sciences;2009-29
3 LI Zhong-ying et al(Hunan Chemical Vocational Technology Institute,Zhuzhou,Hunan 412004);Detection of Total Flavonoids in Panax notoginseng Powder[J];Journal of Anhui Agricultural Sciences;2010-27
4 XU Wei et al(School of Chemical and Biological Engineering,Yancheng Institute of Technology,Yancheng,Jiangsu 224051);Study on Antibacterial Activity and Antioxidant Activity of Total Flavonoids from Reed Leaf[J];Journal of Anhui Agricultural Sciences;2010-29
5 GUO Hai-bin et al(College of Chemistry and Chemical Engineering,Nanjing University of Technology,Nanjing,Jiangsu 210009);Optimization of Microwave-assisted Extraction of the Total Flavonoids from Reed Leaf by Response Surface Methodology[J];Journal of Anhui Agricultural Sciences;2010-29
6 TAN Yong-xia et al(College of Life Science and Technology,Lanzhou University of Technology,Lanzhou,Gansu 730070);Advances in Studies on the Plants of Genus Aconitum[J];Journal of Anhui Agricultural Sciences;2011-24
7 CHEN Fang et al(Department of Chemistry and Environmental Engineering,Jianghan University,Wuhan,Hubei 430056);Determination of Protocatechuic Acid in CORTEX ACANTHOPANACIS Using High Proficiency Liquid Chromatography Coupled with Four-channel UV-visible Detector[J];Journal of Anhui Agricultural Sciences;2011-26
8 CAO Lei et al (College of Life Science,Hebei United University,Tangshan 063000);Cloning and Sequence Analysis of ATPase Beta Subunit Gene from Eleutherococcus senticosus[J];Journal of Anhui Agricultural Sciences;2012-02
9 ZHAO Cheng(Luan Institute for Drug Control,Anhui Province 237000,China);Content determination of syringin in Mie'aoling tablet by HPLC[J];Anhui Medical and Pharmaceutical Journal;2006-12
10 BAI Rui1,WANG Zhen-zhen2 (1.Maanshan Institute for Drug Control,Maanshan 243000,China;2.College of Pharmaceutical Sciences,Zhejiang University,Hangzhou 310058,China);Application of fingerprint in the quality control of traditional Chinese medicine[J];Anhui Medical and Pharmaceutical Journal;2009-12
China Proceedings of conference Full-text Database 5 Hits
1 Jin Zhe-xiong1,Xu Sheng-yan1,SunSu-qin2 1.Pharmic college of Haerbin commercial university and Heilongjiang Province,Haerbin 150076,China 2.Key Laboratory of Bioorganic Phosphorus Chemistry & Chemical Biology(Ministry of Education),Department of Chemistry,Tsinghua University,Beijing 100084,China;Analysis of Acanthopanax senticosus Harms for different parts Using Fourier Transform Infrared Spectroscopy[A];[C];2008
2 ;舒肝解郁胶囊治疗轻中度抑郁症的临床研究[A];[C];2010
3 SUN Qiao, LIU Xiao-jie, MA Qing, ZHANG Li-hua (R&D department of Hangzhou Wahaha Group Company Limited, Hangzhou 310018, China; Department of food science and nutrition, Zhejiang University, Hangzhou 310029, China);Effect of capsule of Hao jing shen on anti-fatigue in rice[A];[C];2007
4 DOU Jian-peng, LIU Zhi-qiang, LIU Shu-ying(1. Laboratory of New Drug Research, Changchun Institute of Applied Chemistry, Chinese Academy of Sciences, Changchun 130022, China; 2. College of Biological and Agricultural Engineering, Jilin University, Changchun 130025, China);Analysis of Two Flavonol Glycoside Isomers by Electrospray Ionization Tandem Mass Spectrometry[A];[C];2004
5 WANG Qian-qian~(1,2),Zhang Yan~(1,3),PI Zi-feng~1,LIU Shu~1,SONG Feng-rui~1, LIU Zhi-qiang~(1*) (1 Changchun Center of Mass Spectrometry,Changchun Institute of Applied Chemistry,Chinese Academy of Sciences,Changchun 130022,China;2 University of the Chinese Academy of Sciences,Beijing 100039,China;3 College of chemistry and pharmaceutical engineering,Jilin Institute of Chemical Technology,Jilin,132022);Protective effect of Acanthopanax leaf extract on cerebral ischemia rats and pharmacokinetic studies of the main components[A];[C];2013
【Secondary Citations】
Chinese Journal Full-text Database 5 Hits
1 Chen Yaozu Chen Nengyu Li Haiquan Zhao Fanzhi and Chen Ning (Department of Chemistry, Lanzhou University, Lanzhou);Application of FAB-MS/MS to Structural Analysis of Saponins[J];Chemical Research In Chinese Universities;1986-10
2 ZHONG Da-Fang*, TIAN Lei, LI Xue-Qing, XU You-Jun (Laboratory of Drug Metabolism and Pharmacokinetics, Shenyang Pharmaceutical University, Shenyang 110015, China);Studies on the Electrospray Ion Trap Mass Spectra of Roxithromycin and Its Metabolites[J];CHEMICAL RESEARCH IN CHINESE UNIVERSITIES;2000-01
3 Zhong Dafang;Chen Xiaoyan;Chen Rendi;Luo Xu(Department of Pharmacy,Shenyang Pharmaceutical University,Shenyang 110015);A STUDY ON THE MAJOR METABOLITE OF ETOFESALAMIDE IN RABBITS[J];JOURNAL OF SHENYANG PHARMACEUTICAL UNIVERSITY;1996-04
4 Zhong Dafang,Gu Jingkai,Jiang Hao,Zhou Hui Laboratory of Drug Metabolism and Pharmacokinetics,Shenyang Pharmaceutical University,Shenyang 110015;Identification of Two Major Metabolites of 3 H 1,2 Dihydro 2 (4 methyl phenylamino)methyl 1 pyrrolizinone in Rabbits Using Electrospray Ion Trap Mass Spectrometry[J];JOURNAL OF SHENYANG PHARMACEUTICAL UNIVERSITY;1999-01
5 LIU Bai-Li, ZHANG Xiao-You~*, WANg Shu-Zhen, WANG Xiu, LI Ya-Qing~* and ZOU Ben-Tian~*(Shenyang College of Pharmaccy, Shenyang; ~*Da Qing No 1 Hospital, Da Qing);SYNTHESIS OF EFUAMIDE[J];Acta Pharmaceutica Sinica;1987-04
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