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《Chemical Journal of Chinese Universities》 2007-01
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Preparation and Structure Characterization of an Alkali-soluble Polysaccharide from Grifola frondosa Mycelium

YU Guang-Li~(*),WANG Ying,ZHAO Xia,GAO Hao-Dong,GUAN Hua-Shi(Marine Drug and Food Institute,Lab of Glycochemistry & Glycotechnology,Ocean University of China,Qingdao 266003,China)  
An alkali-soluble polysaccharide(GFM2A)was extracted by cold sodium hydroxide and further purified by column chromatography from fermented Grifola frondosa mycelium.The structural characterization of GFM2A was confirmed by NaIO_(4) oxidation,Smith degradation,acetolysis,GCMS,IR and NMR techniques.The results showed that GFMZA contain glucose(Glc),mannose(Man)and xylose(Xyl),and their molar ratio was 9∶2∶1.There are six α-1,3-D-Glc and two α-1,3-D-Man in the backbone,and there are two branches in the main chain,and both of them linked to α-1,3-D-Glc residue,one branch contains three β-1,4-D-Glc,another branch contains one α-1,4-D-Xyl.
【Fund】: 国家自然科学基金(批准号:30370345)资助
【CateGory Index】: TQ929
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