Full-Text Search:
Home|Journal Papers|About CNKI|User Service|FAQ|Contact Us|中文
《Chemical Journal of Chinese Universities》 2007-05
Add to Favorite Get Latest Update

Direct Determination of Reserpine in Urine Using Excitation-Emission Fluorescence Combined with Three-dimensional Chemometric Calibration Methodologies

HAN Qing-Juan, WU Hai-Long*, NIE Jin-Fang, XIA A-Lin, ZHU Shao-Hua, ZHANG Yan, YU Ru-Qin(State Key Laboratory of Chemo/Biosensing and Chemometrics, College of Chemistry and Chemical Engineering, Hunan University, Changsha 410082, China)  
The concentration of reserpine in urine was directly and quantitatively measured with the excitation-emission fluorescence(EEM) combined with three-dimensional calibration methodologies. Two calibration methodologies are based on the alternating trilinear decomposition(ATLD) and the self-weighted alternating trilinear decomposition(SWATLD) algorithms, respectively. The satisfactory results of both methods are obtained, when the component number was chosen to be 3(N=3). This experiment is easily carried out without time-consuming and complicated pretreatment. It proved that ATLD and SWATLD based three-dimensional calibration methodologies can be feasible to directly quantify the medical content of reserpine in urine
【Fund】: 国家自然科学基金(批准号:20475014 20435010)资助.
【CateGory Index】: R96
Download(CAJ format) Download(PDF format)
CAJViewer7.0 supports all the CNKI file formats; AdobeReader only supports the PDF format.
【References】
Chinese Journal Full-text Database 6 Hits
1 JIANG Hong,LI Xue-qin,XIE Fa-ping,MAO Xiao-feng and HUANG Jian-qiong(College of Chemistry and Chemical Engineering,Yangtze Normal University,Chongqing 408100);Highly sensitive color reactions of reserpine with rhodamine B and their analytical applications[J];Chinese Journal of Analysis Laboratory;2010-03
2 DU Shu-xin,DU Yang-feng,WU Xiao-li State Key Lab of Industrial Control Technology,Institute of Industrial Process Control,Zhejiang University,Hangzhou 310027,China;The Surface Smoothing Methods for Three-Dimensional Fluorescence Spectrometry Based on Savitzky-Golay Polynomial Smoothing[J];Spectroscopy and Spectral Analysis;2011-02
3 LIU Chun-Yu;WANG Shao-Yan;XU Shu-Ping;XU Wei-Qing;State Key Laboratory of Supramolecular Structure and Materials,Jilin University;College of Science,Changchun University of Science and Technology;;SERS and EEM Fluorescence Spectral Distinction of Sudan Ⅰ and Paprika Red in Food[J];Chemical Journal of Chinese Universities;2013-11
4 JIANG Hong,LI Xue-qin,MAO Xiao-feng,HUANG Jian-qiong(College of Chemistry and Chemical Engineering,Yangtze Normal University,Chongqing 408100,China);Highly sensitive spectrophotometric method for determination of reserpine by victoria blue B[J];Chemical Reagents;2010-06
5 JIANG Hong,PANG Xiang-dong,DENG Qin-xin,HUANG Jian-qiong,LI Xue-qin (Dept.of Chem.and Chem.Eng.Changjiang Normal College,Chongqing 408100,China);Determination of Reserpine by Resonance Rayleigh Scattering Spectrometry[J];Physical Testing and Chemical Analysis(Part B:Chemical Analysis);2010-12
6 WANG Yong-li1,ZHANG Jiang-wei1,WANG Li-hua1,Aodeng Gao-wa2,HUANG Hui-ting1,LI Mei-hong2(1.Institute of Applied Chemistry of Hebei North University,Zhangjiakou 075000,China; 2.College of Chemistry and Chemical Engineering,Inner Mongolia University,Hohhot 010021,China);Research Progress of Fluorimetry in Pharmaceutical Analysis[J];Chinese Journal of Experimental Traditional Medical Formulae;2011-12
【Citations】
Chinese Journal Full-text Database 1 Hits
1 ZHANG Li yao, HUANG Chun bao, YANG Xi, PAN Zu ting * (Department of Chemistry , Wuhan University, Wuhan, 430072);Studies on the Oxidation Reaction of Reserpine by Spectrofluorimetry and Its Analytical Application[J];Journal of Analytical Science;2000-06
【Co-citations】
Chinese Journal Full-text Database 5 Hits
1 WANG Chuan-ping1,SUN Shu-ting2,ZHANG Li-na2,CHEN Xin2,WEI Qin2(1.Shool of Materials Science & Engineering,University of Jinan,Jinan 250022 ,China;2.School of Chemistry & Chemical Engineering,University of Jinan,Jinan 250022,China);Application and Development of the Pharmaceutical Analysis by Photometric Technique[J];Analysis and Testing Technology and Instruments;2007-03
2 LI Shi-feng,WEI Xian-wen,XIAO Yan-ling and ZHU Changqing(School of Chemistry and Materials Science,Anhui Key Laboratory of Functional Molecular Solids,Anhui Normal University,Wuhu 241000);Flow injection analysis of reserpine with inhibited chemiluminescent detection[J];Chinese Journal of Analysis Laboratory;2006-01
3 WENG Wen-ting;XIE Xiao-lan;LUO Shu-mei;College of Chemistry & Life Science,Quanzhou Normal University;;Determination of Lidocaine Hydrochloride Injection by Liquid-Liquid Extraction-Fluorimetry[J];Journal of Analytical Science;2014-06
4 JIANG Hong,LI Xue-qin,MAO Xiao-feng,HUANG Jian-qiong(College of Chemistry and Chemical Engineering,Yangtze Normal University,Chongqing 408100,China);Highly sensitive spectrophotometric method for determination of reserpine by victoria blue B[J];Chemical Reagents;2010-06
5 ZHAO Chang-zhi,DU Hong,LI Ying(Shandong Provincial Key Laboratory of Biochemical Analysis Qingdao University of Science & Technology,Qingdao 266042,China);Determination of reserpine by using an electrochemical oxidation-fluorescence method[J];Journal of Liaoning Normal University(Natural Science Edition);2010-04
【Co-references】
Chinese Journal Full-text Database 10 Hits
1 CHU Ming-jie et al(School of Science,Anhui Agricultural University,Hefei,Anhui 230036);Application of Ionic Liquids in Extraction and Chromatography[J];Journal of Anhui Agricultural Sciences;2008-14
2 CUI Xiang et al(Department of Chemistry,Qinghai Normal University,Xining,Qinghai 810008);Direct Determination of Phenol and Hydroquinone Contents in Environmental Water Based on Three-dimensional Fluorescence Spectroscopy[J];Journal of Anhui Agricultural Sciences;2009-24
3 QIN Ying-Song1, ZHANG Xu2, LI Li1, YU Hong-Li3 1. Department of Pathophysiology, Xuzhou Medical College, Xuzhou, Jiangsu, 221002, P. R. China 2. Department of Otorhinolaryngology, Affiliated Hospital of Xuzhou Medical College, Xuzhou, Jiangsu, 221002, P. R. China 3. Department of Neurobiology, Xuzhou Medical College, Xuzhou, Jiangsu, 221002, P. R. China;Effect of Histamine on Metastasis of Melanoma B16 Cell Xenograft in C57BL/6 Mice[J];Chinese Journal of Cancer;2007-08
4 LV Xing-ping1,TONG Shan-shan2(1.Jiangsu Polytechnic College of Agriculture and Forestry,Jurong 212400,China;2.School of Medicine Jiangsu University,Zhenjiang 212001,China);Determination of Doxorubicin in Plasma by RP-HPLC with Fluorescence Detector[J];Journal of Anhui Science and Technology University;2008-05
5 Cheng Hongyan; Li Suwen; Li Yanping; Zhang Hongqing; Xue Shaobai (Department of Biology, Beijing Normal University, 100875, Beijing, China);ANALYSIS OF FLUORESCENCE EMISSION SPECTRA OF THE ANTICANCER DRUG DOXORUBICIN[J];JOURNAL OF BEIJING NORMAL UNIVERSITY(NATURAL SCIENCE);1999-02
6 Sun Yu?bin,Geng Yu?hong Binzhou Teachers College,Binzhou 256604,China;Development and Prospects of Analytical Chemistry[J];Journal of Binzhou Teachers College;2001-02
7 LIU Qingjun1,2,YE Weiwei1,DU Liping1,YU Hui1,HU Ning1,WANG Ping1,2 1.Biosensor National Special Laboratory,Department of Biomedical Engineering,Key Laboratory of Biomedical Engineering ofNational Education Ministry,Zhejiang University,Hangzhou 310027,China;2.State Key Laboratory of Transducer Technology,Chinese Academy of Sciences,Shanghai 200050,China;Application of Wavelet Transform De-Noising for Neural Cell Based Biosensor[J];Chinese Journal of Sensors and Actuators;2009-11
8 JIN Xiao-ling,GAO Shou-hong,WU Rong,et al;LC-MS/MS in determination of telmisartan concentration in human plasma[J];Academic Journal of Second Military Medical University;2008-12
9 CHENG Si Kun 1, LIU Zhi Guang 1, CAO Yun Xin 1,SONG Jun Feng 2 1Central Laboratory, Faculty of Preclinical Medicine,Fourth Military Medical University, Xi’an 710033, China, 2Institute of Analytical Science, Northwest University;New method in the determination of curcumin by electrochemistry[J];JOURNAL OF THE FOURTH MILITARY MEDICAL UNIVERSITY;2000-02
10 YOU Wen-wei 1 , WU Zhao-hui 2 , TONG Li 2 , XING Xue-feng 21 Teaching and Research Section of Chemistry, Department of Basic Medical Sciences, 2 Key Laboratory of Traditional Chinese Medicine Development, Department of Traditional Chinese Medicine, First Military Medical University, Guangzhou 510515, China;Determination of serum astragaloside in rats fed with Buyanghuanwu dicoction using solid-phase extraction, chemical derivatization and fluorospectrophotometry[J];Journal of First Military Medical University;2003-04
【Secondary References】
Chinese Journal Full-text Database 10 Hits
1 CHENG Li-lin1,2,3,NIE Xiao-bao1,3,4,ZHANG Chang-feng1,2,3,4*,WANG Guo-li3(1.Shandong Key Laboratory of Storage and Transportation Technology of Agricultural Products,Jinan 250103,China; 2.Shandong Institute of Commerce and Technology,Jinan 250103,China; 3.National Engineering Research Center for Agricultural Products Logistics,Jinan 250103,China; 4.College of Food Science of Fujian Agricultural and Forestry University,Fuzhou 350002,China);Research Progress of Detecting Methods for Biogenic Amine in Aquatic Product[J];Shandong Agricultural Sciences;2012-09
2 DU Shu-xin;JIANG Dan-hong;School of Information Science and Engineering,Ningbo Institute of Technology,Zhejiang University;;Utilizing 3-D first-order derivative fluorescence spectrometry to detect aflatoxin in foods based on STM[J];Journal of Optoelectronics.Laser;2014-03
3 YANG Ren-xin;YANG Yan;YUAN Jing-jing;School of Mathematical and Statistics Sciences,Guangxi Teachers Education University;;The Research and Progress of Hyperspectral Image Preprocessing Method[J];Journal of Guangxi Teachers Education University(Natural Science Edition);2015-01
4 DU Shu-xin1,SHEN Jin-chang1,YUAN Zhi-bao2 (1.State Key Lab of Industrial Control Technology,Institute of Industrial Process Control,Zhejiang University,Hangzhou 310027,China;2.Hainan Entry-Exit Inspection and Quarantine Bureau,Haikou 570311,China);Multi-way partial least squares modeling for three-dimensional fluorescence spectrometry[J];Laser Journal;2012-01
5 DU Shu-xin;WU Yuan-qing;WANG Jian;Ningbo Institute of Technology,Zhejiang University;Shanghai Entry-Exit Inspection and Quarantine Bureau;;COD Detection in Wastewater Treatment Based on Three-dimensional Fluorescence Spectrometry[J];Control and Instruments in Chemical Industry;2013-08
6 Sun Jun;Zhang Meixia;Mao Hanping;Li Zhengming;Yang Ning;Wu Xiaohong;Key Laboratory of Modern Agricultural Equipment and Technology,Ministry of Education,Jiangsu University;School of Electrical and Information Engineering,Jiangsu University;;Identification of Pesticide Residues on Mulberry Leaves Based on Hyperspectral Imaging[J];Transactions of the Chinese Society for Agricultural Machinery;2015-06
7 WANG Mei-dan1,GAO Yan2,ZHAO Bo-nian2(1.College of Pharmacy,Shandong University of Traditional Chinese Medicine,Jinan 250355,China;2.Shandong Academy of Traditional Chinese Medicine,Jinan 250014,China);Progress on Application of Fluorimetry in Pharmaceutical Research[J];Food and Drug;2013-01
8 LIU Min-fa;ZHANG Ling-biao;HE Jian-guo;HE Xiao-guang;LIU Gui-shan;WANG Song-lei;School of Agriculture,Ningxia University;;Study on non-destructive detection of pesticide residues on Lingwu long jujubes' surface using hyperspectral imaging[J];Food & Machinery;2014-05
9 LI Xiao-mei 1,KANG Zhi-ying 1,LIANG Yong 1,MA Yin-lian 2,YU Ding-rong 2(1.Guangzhou Xiangxue Pharmaceutical Co.LTD,Guangzhou 510663,China;2.Institute of Chinese Materia Medica,China Academy of Chinese Medical Sciences,Beijing 100700,China);Determination of Salvianolic Acid B in Zhongfenghuichun Capsule by HPLC[J];Chinese Journal of Experimental Traditional Medical Formulae;2013-13
10 LI Xiao-mei 1,LIANG Yong 1,KANG Zhi-ying 1,WANG De-xiu 1,CAI Chun-ling 1,MA Yin-lian 2,YU Ding-rong 2(1.Guangzhou Xiangxue Pharmaceutical Co.Ltd.,Guangzhou 510663,China;2.Institute of Chinese Materia Medica,China Academy of Chinese Medical Sciences,Beijing 100700,China);Determination of Hydroxyacetophenone in Qingganlidan Oral Solution[J];Chinese Journal of Experimental Traditional Medical Formulae;2013-17
【Secondary Citations】
Chinese Journal Full-text Database 2 Hits
1 Li Liqing, Yang Minli, Feng Manliang, Lu Jiuru (Department of Chemistry, Shaanxi Normal University, Xi'an 710062);Determination of Reserpine by Flow-injection Chemiluminescence Analysis[J];Chinese Journal of Analytieal Chemistry;1998-03
2 Yang Huifang 1, Liu Yanfang 2, Wang Zhihua 2 and Ding Tianhui 2 1(Hebei Medical University, Shijiazhuang, 050017) 2(Hebei University, Baoding, 071002);Determination of Hydrophobic Pharmaceutical:Tablet of Reserpine Compound by Capillary Zone Electrophoresis[J];CHINESE JOURNAL OF CHROMATOGRAPHY;1998-02
©2006 Tsinghua Tongfang Knowledge Network Technology Co., Ltd.(Beijing)(TTKN) All rights reserved