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《Chemical Journal of Chinese Universities》 2007-05
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Direct Determination of Reserpine in Urine Using Excitation-Emission Fluorescence Combined with Three-dimensional Chemometric Calibration Methodologies

HAN Qing-Juan, WU Hai-Long*, NIE Jin-Fang, XIA A-Lin, ZHU Shao-Hua, ZHANG Yan, YU Ru-Qin(State Key Laboratory of Chemo/Biosensing and Chemometrics, College of Chemistry and Chemical Engineering, Hunan University, Changsha 410082, China)  
The concentration of reserpine in urine was directly and quantitatively measured with the excitation-emission fluorescence(EEM) combined with three-dimensional calibration methodologies. Two calibration methodologies are based on the alternating trilinear decomposition(ATLD) and the self-weighted alternating trilinear decomposition(SWATLD) algorithms, respectively. The satisfactory results of both methods are obtained, when the component number was chosen to be 3(N=3). This experiment is easily carried out without time-consuming and complicated pretreatment. It proved that ATLD and SWATLD based three-dimensional calibration methodologies can be feasible to directly quantify the medical content of reserpine in urine
【Fund】: 国家自然科学基金(批准号:20475014 20435010)资助.
【CateGory Index】: R96
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