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《Chemical Journal of Chinese Universities》 2012-05
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Design and Preparation of SiO_2/SiO_2-TiO_2 Antireflective Coating with Excellent Environmental Resistance

YE Long-Qiang,ZHANG Xin-Xiang,XIAO Bo,YE Hai-Ping,JIANG Bo (Key Laboratory of Green Chemistry & Technology,Ministry of Education,College of Chemistry, Sichuan University,Chengdu 610064,China)  
Double-layer antireflective(AR) coatings on K9 glass with excellent environmental resistance and abrasion-resistance were designed and prepared.Using tetraethylorthosilicate(TEOS) and titanium tetraisopropoxide(TTIP) as precursor,respectively,SiO 2 and TiO 2 sols were prepared via sol-gel process with hydrochloric acid as catalyst.SiO 2-TiO 2 composite films were prepared by mixing the SiO 2 and TiO 2 sols and then dip-coating on the substrates.The refractive indices of the composite films were controlled by adjusting the SiO 2/TiO 2 ratio and the thickness was controlled by adjusting the dip-coating speed.It was found that the maximum transmittance of the double-layer AR coatings reached 99.9% and could be adjusted to match a specific wavelength.The transmittance did not decrease after abrasion test,indicating an excellent abrasion-resistance of the AR coating.Hydroxyl terminated hexamethyldisiloxane(HMDS) treatment was further performed to improve the hydrophobicity,the environmental resistance and durability of the AR coatings.
【Fund】: 中央高校基本科研业务费(批准号:2010SCU23003)资助
【CateGory Index】: TB383.2
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