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《CHEMICAL RESEARCH IN CHINESE UNIVERSITIES》 1999-07
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Studies on Preparation and Anion Exchange Capacity of Mg Fe LDHs Nanoparticles

SU Yan Lei, HOU Wan Guo *, SUN De Jun LIU Shang Ying, Zhang Chun Guang (Key Laboratory for Colloid and Interface Chemistry of the Ministry of Education, Shandong University, Jinan, 250100)  
The nanoparticles of magnesium ferric layered double hydroxides(Mg Fe LDHs) were synthesized by coprecipition method, and their shape, chemical composition, crystal structure, anion exchange capacity and the effects of the n (Mg)∶ n (Fe) in raw material on these properties were studied by transmission electron microscope, chemical analysis and X ray diffraction etc.. It was found that the Mg Fe LDHs particles were plate like nanoparticles, and their chemical compositions are basically consistent with the compositions of raw materials. In the range of n (Mg)∶ n (Fe) of 2∶1~4∶1, the Mg Fe LDHs has the same layered crystal structure as hydrotalcite which belongs to the hexagonal system. With increasing of n (Mg)∶ n (Fe) in the chemical compositions of the samples from 2∶1 to 4∶1, the particle size of the samples increases from 37.9 nm to 61.2 nm. The lattice constant, a , of hexagonal cell decreases from 0.317 nm to 0.310 nm and the lattice constant, c , of hexagonal cell increases from 2.380 nm to 2.412 nm. The basal spacing of the Mg Fe LDHs increases from 0.793 nm to 0.804 nm. The anion exchange capacity of the Mg Fe LDHs increases from 0.52 mmol/g to 1.82 mmol/g.
【Fund】: 国家自然科学基金 山东省自然科学基金
【CateGory Index】: O647.2
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