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《Academic Journal of Guangdong College of Pharmacy》 2005-02
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Synthesis of ethyl p-methoxy cinnamate

ZHANG Hong,DING Ying-hong,LI Ruo-qi(Department of Organic Chemistry,Guangdong College of Pharmacy, Guangzhou 510240,China)  
An efficient synthesis of p-methoxy cinnamic acid, a key intermediate for ethyl p-methoxy cinnamate, was developed on the basis of Knoevenagel condensation of p-anisaldehyde with a catalytic amount of ammonium acetate under microwave irradiation in the yield of 87.8%. Then, p-methoxy cinnamic acid obtained was converted to ethyl p-methoxy cinnamate by esterification using p-toluenesulfonic acid as catalyst in excellent yield (91.0%). The structures of p-methoxy cinnamic acid and ethyl p-methoxy cinnamate were confirmed by IR and ~1H-NMR.
【CateGory Index】: R914.5
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【References】
Chinese Journal Full-text Database 9 Hits
1 LIMAO Cai-rang et al(Chemistry Department of Nationality Teacher College,Qinghai Normal University,Xining,Qinghai 810008);Study on Extraction Conditions of Ethylp-methoxy Cinnamate from Kaempferia galanga L.[J];Journal of Anhui Agricultural Sciences;2008-33
2 LI Yu,HUANG Guo-chao(Guangdong Industry Technical College,Guangzhou 510300,China);Microwave Assisted Synthesis and Application of Cinnamic Esters on Packaging Materials[J];Packaging Engineering;2007-02
3 Zhang Chao,Wu Aiping,Deng Yufeng(Basis College,Guangzhou Medical College,Guangzhou 510182,China);Study on the Catalytic Synthesis of Ethyl p-methoxy Cinnamate by KF/A1_2O_3 Solid Superbase[J];Guangdong Chemical Industry;2010-04
4 ZENG Qing-you (1 Department of Chemical Engineering of Material College,Huaqiao University,Quanzhou 362021,China);New process for the synthesis of 2-ethyihexyl p-methoxy cinnamate[J];Chemical Engineer;2007-10
5 ZENG Qin-you1,2,3,ZENG Ming-rong1,XU Rui-an2,3(1.College of Material Science and Engineering,Huaqiao University,Quanzhou 362021,Fujian,China;2.Molecular Medicine Engineering Research Centre of Ministry of Education,Quanzhou 362021,Fujian,China;3.Institute of Molecular Medicine,Huaqiao University,Quanzhou 362021,Fujian,China);One-pot Synthesis of Ethyl p-Methoxycinnamate[J];Fine Chemicals;2008-02
6 LIN Yan,ZHOU Wen-fu(Department of Chemistry and Bio-Engineering,Sanming University,Sanming 365004,China);Synthesis of ultraviolet absorbent iso-amyl p-methoxycinnamate catalyzed by bamboo carbon[J];Applied Chemical Industry;2009-11
7 HUANG Li1,LI Yu1,2,ZHANG De-zhi1*(1.School of Pharmacology,Guangdong College of Pharmacology,Guangzhou 510006,China;2.Department of Chemical Engineering,Guangdong Industry Technological College,Guangzhou,510300,China);The Review of Microwave Assisted Synthesis of Aromatic Esters[J];Lishizhen Medicine and Materia Medica Research;2008-03
8 LI He;ZENG Qing-you;College of Chemical Engineering,Huaqiao University;;One-pot synthesis of isoamyl p-methoxycinnamate[J];Applied Chemical Industry;2013-10
9 ZHANG Guang-gui, ZHANG Ying-peng, GOU Guo-jun, SU Ce~* (Institute of Organic & Medicinal Chemistry, School of Petrochemical Engineering, Lanzhou University of Technology, Lanzhou 730050);Preparation of 3,4,5-Trimethoxycinnamic Acid[J];Chinese Journal of Pharmaceuticals;2007-11
【Citations】
Chinese Journal Full-text Database 4 Hits
1 WANG Wei hong, FAN Jun yuan, CHENG Xin yuan, LUO Yi ming (Department of Chemistry Hunan Medical University, Changsha 410078, China);Synthesis of Methyl Cinnamate and Ethyl Cinnamate Using p-Toluene Sulforic Acid as Catalyst[J];Hunan Chemical Industry;2000-06
2 ZHANG Hong,WU Yi-qin,YU Kun-song,SHI Yu-xuan(Department of Pharmacy,Guangdong College of Pharmacy,Guangzhou 510224,China);Synthesis of p-methoxy cinnamic acid under microwave irradiation without solvent[J];Detergent & Cosmetics;2004-12
3 Jin Jishu,Du Shuhu (Ankui Institute of Medical Sciences,Hefei,230061);SYNTHESIS OF ETHYL P-METHOXYCINNAMATE,THE MAJOR ANTIFUNGAL PRINCIPLE OF CURCUMA ZEDOARIA ROSCOE[J];Natural Product Research and Development;1994-01
4 Zhang Hong Ou Guoyong (*Department of Pharmacy, Guangdong College of Pharmacy, Guangzhou 510224) (Department of Chemical Engineering, Guangdong University of Technology, Guangzhou 510090);Progress in the Synthesis of p-Methoxy Cinnamate as Sun-screening Agent[J];Flavour Fragrance Cosmetics;2001-03
【Co-citations】
Chinese Journal Full-text Database 10 Hits
1 YANG Jie,SONG Ji-mei,FANG Fang(College of Chemistry and Chemical Engineering,Anhui University,Hefei 230039,China);Determination of caffeine by ATR-infrared spectroscopy[J];Journal of Anhui University(Natural Sciences);2009-01
2 YANG Yun-shang et al(Institute of Organic Pharmaceutical Chemistry,School of Petrochemical Engineering,Lanzhou University of Technology,Lanzhou,Gansu 730050);Synthesis of New Nutritional Additive Neotame-Calcium Chelate[J];Journal of Anhui Agricultural Sciences;2011-16
3 LI Wen--xia;NIE Su--shuang;LU Xao-lan Department of Material Engineering, Beijing Institute of Clothing Technolgy, Beijing 100029, China;Modification of Disperse Dye for Cotton Transfer Printing[J];Journal of Beijing Institute of Clothing;2004-02
4 JIN Shao-hua1,CHEN Shu-sen1,LEI Xiang-dong2(1.School of Material Science and Engineering,Beijing Institute of Technology, Beijing 100081,China;2.The 31nd Institute,China Aerospace Science & Industry Corpration,Beijing 100074,China);Investigation of Adducts of HNIW with DMF and DMSO[J];Acta Armamentarii;2008-01
5 ZHU QiuJin~(1,2) GU XiaoHong~1 TANG Jian~(1) WANG LinXiang~1 FENG Yu~1 LI GaoYang~1(1.Key Laboratory of Food Science and Safety,Ministry of Education,Southern Yangtze University,Wuxi Jiangsu 214036;2.School of Life Science,Guizhou University,Guiyang Guizhou 550025;3.Testing & Analysis Centre,Southern Yangtze University,Wuxi Jiangsu 214036,China);Interaction of 17β-estradiol and its structural analogues with functional monomers[J];Journal of Beijing University of Chemical Technology(Natural Science Edition);2007-01
6 Lin Shijing1 Tong Laga1 Ding Hong1Sun Yangzhao2 Lian Huawen1(1.Department of Chemical Engineering,Beijing Institute of Petro-chemical Technology,Beijing 102617,China; 2.Ministry of Environmental Protection of the Perple's Republic of China,Beijing 100035,China);Synthesis of p-methoxy-cinnamic Acid Under Microwave Irradiation[J];Journal of Beijing Institute of Petro-Chemical Technology;2009-03
7 YAN Wei-wei1,YUAN Xin-qiang2,SHI Bin2,XU Lei2(1.Department of Earth Sciences,Sun Yat-Sen University,Guangzhou 510275,China;2.Gemmological Institute,China University of Geosciences,Wuhan 430074,China);Quantitative Test Method on Content of Wax in Jadeite Jade[J];Journal of Gems & Gemmology;2008-04
8 LI Yu,HUANG Guo-chao(Guangdong Industry Technical College,Guangzhou 510300,China);Microwave Assisted Synthesis and Application of Cinnamic Esters on Packaging Materials[J];Packaging Engineering;2007-02
9 YU Shan-xin1,WEN Rui-ming2,YOU Pei-qing2(1.College of Chemistry and Chemical Engineering,Hunan Normal University,Changsha 410081,China; 2.Department of Chemistry and Environmentally Engineering,Hunan City University,Yiyang 413000,China);Research progress of synthesis of ethyl cinnamate[J];Journal of Hunan University of Arts and Science(Natural Science Edition);2011-01
10 HAN Hong-mei1,NAN Yan-ping1,ZHAO Zhi-min1,2,ZHU Long-ping1,CEN Shan2,HE Guo-rui2,YANG De-po1,2(1.Institute of Natural Products and Chinese Medicine,School of Pharmaceutical Sciences,Sun Yat-sen University,Guangzhou,Guangdong 510006,China;2.Guangdong Technology Research Center for Advanced Chinese Medicine,Guangzhou,Guangdong 510006,China);Preparation and measurement of antimicrobial activity of ethyl-p-methoxycinnamate[J];China Surfactant Detergent & Cosmetics;2011-04
China Proceedings of conference Full-text Database 5 Hits
1 Zhang Yan,Liu Yujian,Wang Jinggang (School of Materials Science and Engineering,East China University of Science and Technology,Shanghai 200237);Synthesis and Characterization of Allyl Phenyl Ether and 2-Allyl Phenol[A];[C];2006
2 Yan Zan-kai (Department of Chemistry, Hanshan Normal College, Chaozhou 521041);Catalytic Synthesis of Ethyl Cinnamate with TBAB[A];[C];2010
3 HAN Hong-mei~1,HUANG Miao-ling~1,ZHUO Li-mei~1,HUANG Yong-ping~1, ZHU Long-ping~1,MEI Jia-qi~1,YANG De-po~(1**) 1 Institute of TCM and Natural Medicine,School of Pharmaceutical Sciences,Sun Yat-sen University, Guangzhou,Guangdong Province 510006,China 2 Guangzhou Xin De Spice Technology Co.,Ltd Guangzhou,Guangdong Province 510430,China;The Extraction and Enrichment of ethyl-P-methoxycinnamate from Rhizoma Kaempferiae by Supercritical Fluid Extraction and Molecular Distillation[A];[C];2010
4 Zhu Xiao-hu,Zhao Xin,Qiao Ai-xin,Tang Jun(The Center of Analysis and Measurement of Xinjiang University,Urumqi 830046);NMR Studies on the Liquefaction Oil Composition of zhongdong Coal by Hydrogenation[A];[C];2012
5 CHEN Cong-jie~(1,2),ZHANG Ming~1,WANG Chun-hong~(2*),MA Chong-qi~2 (1.Beijing Institute of Aeronautical Materials,Beijing 100095,China; 2.Tianjin Polytechnic University,Tianjin 300387,China);STUDY ON SURFACE PHYSICOCHEMICAL PROPERTIES OF FOUR TYPES OF CARBON FIBERS[A];[C];2012
【Co-references】
Chinese Journal Full-text Database 10 Hits
1 Zhang Yu Zou Guolin Peng Shaojun (College of life sciences, Wuhan University, Wuhan 430072,China);The Research Progress of Epigallocatechin Gallate[J];AMINO ACIDS & BIOTIC RESOURCES;1998-04
2 LI Yu~(1,2),KUANG Shou-min~2,LI Shuang~2,HU Jing-chao~2,HUANG Guo-chao~2,ZHANG Jian~2,LI Li-hong~2,LI Guo-liang~2(1.Sun Yat-Sen University,Guangzhou 510275, China; 2.GuangDong Industry Technical College,GuangZhou 510300,CHina);Studies on the Determination of Flavonoid in Juncus Effuses L.[J];Packaging Engineering;2006-05
3 YIN Yanqiu,LIU Yun(College of Chemistry and Environment,Beijing Technology and Business University,Beijing100037,China);Perspective of sun-protecting agents[J];China Surfactant Detergent & Cosmetics;2003-03
4 YUAN Xingdong 1,2*, SHEN Jian 1, LI Guohui 2, Ji-Man KIM 3, Sang-Eon PARK 3 (1 Department of Petrochemical Technology, Fushun Petroleum Institute, Fushun 113001, Liaoning, China; 2 Institute of Coal Chemistry, The Chinese Academy of Sciences, Tai;Preparation and Catalytic Activity of SBA-15 Mesoporous Silica Functionalized with Sulfonic Acid Groups[J];Chinese Journal of Catalysis;2002-05
5 ZHANG Ding-lin~(1,2),WEI Xi-wen~1,LIU Yi-min~2(1.College of Chemistry,Chongqing University,Chongqing 400044;2.Dept.of Chemistry,Third Military Medical University,Chongqing 400038,China);Density Functional Theory on Dimethyl Carbonate as Methylation Reagent[J];Journal of Chongqing Normal University(Natural Science Edition);2006-04
6 YU Shan-xin; ZHANG Lu-xi; ZEN You-lin (College of Chemistry and Chemical Engineering, Hunan Normal University, Changsha, 410081, China);Catalytic Synthesis of Ethyl Cinnamate with Ammanum Ferric Sulfate[J];JOURNAL OF HUNAN EDUCATIONAL INSTITUTE;2000-02
7 ZHANG Jing-qing,YAN Jie-min(Department of Chemistry, Foshan University, Foshan 528000,China);New process for synthesis of benzyl cinnamate[J];Journal of Foshan University(Natural Science Edition);2003-04
8 YU Shan xin,ZHANG Lu xi,ZENG Ying(Department of Chemistry, Hunan Normal Univeristy, Changsha 410081, China );Catalytic synthesis of n propyl cinnamate with ferric chloride[J];JOURNAL OF FOSHAN UNIVERSITY(NATURAL SCIENCE EDITION);1999-03
9 REN Li-guo,GAO Wen-yi,ZHAO Chong-feng(School of Petrochemical Technology, Liaoning University of Petroleum & Chemical Technology,Fushun Liaoning 113001, P.R.China);Synthesis of Cinnamic Acid From Styrene and Carbon Tetrachloride[J];;2005-01
10 Meng Qingmin Zhang Aili(Department of Petrochemical Engineering, Fushun Petroleum Institute, Liaoning Fushun 113001)Gao Jun(Fushun Aluminium Plant Technical School, Liaoning Fushun 113001);Synthesis of Cinnamic Acid Lauric Anhydride by the Pd Catalyst[J];JOURNAL OF FUSHUN PETROLEUM INSTITUTE;1998-02
【Secondary References】
Chinese Journal Full-text Database 10 Hits
1 WANG Rui et al(Department of Chemistry,Zhaotong Teacher's College,Zhaotong,Yunnan 657000);Antioxidation of Kaempferia galanga L. Extracts on Edible Oils[J];Journal of Anhui Agricultural Sciences;2010-26
2 HE Mei et al(Chemistry Department of Zhaotong Teachers College,Zhaotong,Yunnan 657000);Research Advance of Kaempferia galanga L.[J];Journal of Anhui Agricultural Sciences;2010-26
3 LI Yu1,2,HUANG Li2,ZHANG De-zhi2,TAO Wen-cheng1(1.Department of Chemical Engineering,Guangdong Industry Technical College,Guangzhou 510300,China;2.College of Pharmacy,Guangdong College of Pharmacy,Guangzhou 510006,China);Study on microwave assisted synthesis of n-butyl cinnamate catalyzed by macroporous resin[J];China Surfactant Detergent & Cosmetics;2008-01
4 ZHANG Tian-zhu,ZENG Yong,ZHU Fu-wei,HU Mei-ying,WENG Qun-fang(Laboratory of Insect Toxicology,South China Agricultural University & Key Laboratory of Pesticides and Chemical Biology Ministry of Education of P.R.China,Guangzhou 510642,China);Isolation and Identification of Nematicide Component from Kaempferia galanga L.[J];Acta Botanica Boreali-Occidentalia Sinica;2010-12
5 Zhang Chao,Wu Aiping,Deng Yufeng(Basis College,Guangzhou Medical College,Guangzhou 510182,China);Study on the Catalytic Synthesis of Ethyl p-methoxy Cinnamate by KF/A1_2O_3 Solid Superbase[J];Guangdong Chemical Industry;2010-04
6 Xue Ping,Chen Yu,Ou Can-xian,Lin Jinbin,Pan Jingxing(Department of Chemical Engineering,Guangdong Industry Technical College,Guangzhou 510300,China);Study on Microwave Assisted Synthesis of n-butyl Cinnamate Catalysized by Macroporous Resin[J];Journal of Guangdong Industry Technical College;2008-04
7 LIN Chunxiao1,CAI Zhishun2,SU Limin2,WANG Liyun2,LU Xiaofei2,GAO Huijuan2,LI Yu2(1.NanShan Maternal-Child Hospital,ShenZhen 518052,China;2.Department of Chemical Engineering,Guangdong Industry Technical College,Guangzhou 510300,China);Study on Enlarged Processes of Microwave Assisted Synthesis of Cinnamon Esters Catalysized by Macroporous Resin(Ⅱ)[J];Guangdong Trace Elements Science;2008-11
8 Yao Xuancheng;Shuai Jun;Huang Dongxia;Chen Chunxia;Liu Yi;Zeng Hongyao;College of Chemistry,Leshan Normal University;;Study on Basic Hydrolysis of Ethyl Coumarin-3-carboxylate[J];Guangdong Chemical Industry;2013-24
9 YANG Xiao-jun(College of Chemistry and Chemical Engineering,Yan′an University,Yan′an 716000,China);Study on the Chemical Constituents of the Mycelia of Micropolyspora sp.[J];Chemistry & Bioengineering;2011-05
10 ZENG Hong-yao*,LU Xiao-dong,XU Ting,SUN Guo-feng(College of Chemistry and Biology Science,Leshan Normal University,Leshan 614000,China);Synthesis of ethyl coumarin-3-carboxylate catalyzed by L-proline in PEG-400[J];Chemical Research and Application;2012-05
【Secondary Citations】
Chinese Journal Full-text Database 5 Hits
1 Yu Shanxin(Department of Chemistry,Hunan Normal University,Changsha410081),Yu Chaoyuan (Zhounan Medial School,Changsha410005);Catalytic synthesis or ethyl cinnamate with ferric chloride[J];CHEMICAL REAGENTS;1996-04
2 Jin Jishu,Du Shuhu (Ankui Institute of Medical Sciences,Hefei,230061);SYNTHESIS OF ETHYL P-METHOXYCINNAMATE,THE MAJOR ANTIFUNGAL PRINCIPLE OF CURCUMA ZEDOARIA ROSCOE[J];Natural Product Research and Development;1994-01
3 Xu Liang (Beijing Daily Chemical New Materials and Basic Science Laboratory 100061);An Approach on the Formulation Technology and Future Development of Sun Care Cosmetics[J];FLAVOUR FRAGRANCE COSMETICS;1999-04
4 Zhang Hong Ou Guoyong (*Department of Pharmacy, Guangdong College of Pharmacy, Guangzhou 510224) (Department of Chemical Engineering, Guangdong University of Technology, Guangzhou 510090);Progress in the Synthesis of p-Methoxy Cinnamate as Sun-screening Agent[J];Flavour Fragrance Cosmetics;2001-03
5 WANG, Guan-Wu WANG, Bao-Liang (Department of Chemistry, University of Science and Technology of China, Hefei 230026);Uncatalyzed and Solvent-Free Knoevenagel Condensation under Microwave Irradiation or Heating Conditions[J];Chinese Journal of Organic Chemistry;2004-01
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