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《ACTA POLYMERICA SINICA》 1999-03
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KINETICS OF ISOTHERMAL CRYSTALLIZATION FOR\=NYLON 6/MONTMORILLONITE NANOCOMPOSITES

LIU Limin, ZHU Xiaoguang, QI Zongneng\= (State Key Laboratory of Engineering Plastics,Institute of Chemistry,Chinese Academy of Sciences,Beijing\ 100080)  
The kinetics of isothermal crystallization of nylon 6/montmorillonite nanocomposites with different content of montmorillonite prepared by melt intercalation process has been investigated by DSC.It is shown that the presence of nanometer montmorillonite particles displays a high propensity to nucleate Nylon 6 crystallization,enhance the crystallization rate of Nylon 6,reduce the surface free energies of the developing crystals and improve the behavior of isothermal crystallization of Nylon 6 dealt with the Avrami and Hoffman theories.The crystallization process of Nylon 6 is composed of two stages:the spherulite growth stage and the spherulite nucleation stage.With the increment of the clay content in the Nylon 6/montmorillonite nanoconposites,the crystallization rate parameter k decreases and the surface free energy of the Nylon 6 crystals increases;the spherulite growth stage would become the main stage of the crystallization process in place of the spherulite nucleation stage.\=
【Fund】: 国家自然科学基金
【CateGory Index】: TQ323.6
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