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《Arid Environmental Monitoring》 2009-02
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Analysis of Phthalates(PAEs) in Soil Using GC/MS Coupled with Accelerated Solvent Extraction and Gel Permeation Chromatographic Purification

SHAO Chang-ming,ZHU Wen-ping(Gansu Environmental Monitoring Center,Lanzhou Gansu 730030,China)  
The analytical method of six types of phthalates(PAEs) compounds in soil using capillary column gas chromatography-mass spectrometry with selected ion monitor(GC-MS-SIM) coupled with accelerated solvent extraction and gel permiation chromatographic purification has been established.The results indicated that the determination limit of six types of PAEs in soil ranged from 14 μg/kg to 42 μg/kg with 65.5%~104.4% average recoveries and 5.19%~9.61% relative standard deviation.The method with the advantages of simple operation,good purification and more friendly to environment will be of immense benefit for practical applications.
【CateGory Index】: X131.3
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