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《High Technology Letters》 2001-08
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Surface Sulfonation of Silk Fibroin Film by Plasma Treatment and in vitro Antithrombogenicity

Gu Jinwei, Yang Xinlin, Wang Liyong, Zhu Hesun (Research Center of Materials Science, Beijing Institute of Technology, Beijing 100081)  
Bombyx mori silk fibroin (SF) film was treated by plasma processes with SO 2 gas to introduce functional groups on the surface of film. Meanwhile, functional groups were also introduced by the reaction of 1,3 propane sultone with amine sites on the surface of silk fibroin film which were produced by NH 3 gas plasma. XPS and ATR FTIR were used to analyze the surface chemical elements. The in vitro antithrombogenicity was determined by the method of APTT, TT and PT test. It was shown that sulfonic group was covalently grafted on the surface of the films after both kinds of treatments, and the antithrombogencity of the films was increased remarkably due to the surface sulfonation.
【Fund】: 国家“973”计划资助项目 (G19990 64 7)
【CateGory Index】: R318.08
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