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《JOURNAL OF FUNCTIONAL MATERIALS》 1999-05
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Preparation of TiO_2 Ultrafine Particles by Water-in-oil Microemulsion Reaction

SHI Liyi; HU Yingyu; ZHANG Jianping;( 1 School of Chemistry and Chemical Engineering, Shanghai University, Shanghai, 200072, China);FANG Dingye; LI Chunzhong (2East China university of Science and Technology, Shanghai, 200237, China)  
The precursor of TiO2 ultrafine particles, titanium hydroxides, were synthesized in nonionic water in oiI (W/O) microemulsions.The red - shifted peak appeared in the UV - VIS spectrum when the vatue of co (ω= [H2O]/ [surfactant] ) or reaction time increased.The hydroxide particles were calcined at 650℃ and 1000℃ to form TiO2 ultrafine particles. The measurement of IR, XRD, TEM, EDS, BET surface area were used to characterized the particles. The results showed that the samples calcined at 650℃ were anatase Phase, and the average grain size and BET specific surface area were 24. 6nm and 53. 8m2/g respectively, and the samples calcined at 1000℃ were rutile phase, the average grain size and BET specific surface area were 53. 5nm and 20. 3m2/g respectively.
【CateGory Index】: TB383
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