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《Journal of Functional Materials》 2005-08
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On the pyrite(FeS_2) thin films prepared by sulfurizing the electrodeposited precursive films at different sulfur vapor pressure

HOU Ling,LIU Yan-hui,MENG Liang (Institute of Metal Materials,Zhejiang University,Hangzhou 310027,China)  
The polycrystalline FeS_2 thin films were prepared by thermal sulfurizing the electrodeposited precursive films.The effect of sulfur vapor pressure on the microstructure and crystal characterization of the films were investigated.The sulfurizing reaction of the precursive Fe_3O_4 prepared by electrodepositing was insufficient and results in the presence of a combined structure of FeS_2 and Fe_3O_4 at low sulfur vapor pressure.The precursive Fe_3O_4 was completely transformed into the polycrystalline FeS_2 thin films by sulfurization annealing at the sulfur vapor pressures higher than 20kPa.The precursive films prepared by electrodepositing show a porous and loose structure.The morphology of the FeS_2 films can change from the porous and loose structure into the smooth and compact structure with increasing the sulfur vapor pressure.The crystallite size of the FeS_2 films shows an insignificant change with the sulfur vapor pressure but the lattice constant slightly decreases as the sulfur vapor pressure increases from 5 to 40kPa.
【Fund】: 国家自然科学基金资助项目(50071056)
【CateGory Index】: TN304.2;
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【Citations】
Chinese Journal Full-text Database 1 Hits
1 Huang Wei,Meng Liang (Institute of Metal Materials,Zhejiang University,Hangzhou 310027,China);RESEARCH AND DEVELOPMENT OF PHOTOELECTRICAL CHARACTERIZATIONS OF FeS_2(PYRITE)THIN FILMS[J];Acta Energiae Solaris Sinica;2001-04
【Co-citations】
Chinese Journal Full-text Database 10 Hits
1 WANG Pei~1, ZHAO Gao-ling~1, SHEN Feng-ying~2, HAN Gao-rong~1 Science and Engineering, Zhejiang University, Hangzhou 310027,China;2. Hangzhou Glass Group Co., Ltd, Hangzhou 310022,China);Preparation and characteristic of Fe_xS_y/TiO_2 composite material film[J];Journal of Functional Materials;2004-04
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3 ZHANG Chen-ning1,HU Zhi-qiang1,LIU Li-hong1,YU Xian-xian1,GAO Yan1,Masayuki Okuya2,Shoji Kaneko2(1.Department of Materials Science and Engineering,Dalian Institute of Light Industry,Dalian 116034,China;2.Department of Materials Science Shizuoka University,3-5-1 Johoku,Hamamatsu-shi,Shizuoka 432-8561,Japan);Photoelectric performance of FeS_2/TiO_2 composite thin films[J];Journal of Functional Materials and Devices;2007-02
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