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《Journal of Functional Materials》 2005-08
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On the pyrite(FeS_2) thin films prepared by sulfurizing the electrodeposited precursive films at different sulfur vapor pressure

HOU Ling,LIU Yan-hui,MENG Liang (Institute of Metal Materials,Zhejiang University,Hangzhou 310027,China)  
The polycrystalline FeS_2 thin films were prepared by thermal sulfurizing the electrodeposited precursive films.The effect of sulfur vapor pressure on the microstructure and crystal characterization of the films were investigated.The sulfurizing reaction of the precursive Fe_3O_4 prepared by electrodepositing was insufficient and results in the presence of a combined structure of FeS_2 and Fe_3O_4 at low sulfur vapor pressure.The precursive Fe_3O_4 was completely transformed into the polycrystalline FeS_2 thin films by sulfurization annealing at the sulfur vapor pressures higher than 20kPa.The precursive films prepared by electrodepositing show a porous and loose structure.The morphology of the FeS_2 films can change from the porous and loose structure into the smooth and compact structure with increasing the sulfur vapor pressure.The crystallite size of the FeS_2 films shows an insignificant change with the sulfur vapor pressure but the lattice constant slightly decreases as the sulfur vapor pressure increases from 5 to 40kPa.
【Fund】: 国家自然科学基金资助项目(50071056)
【CateGory Index】: TN304.2;
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