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《Journal of Functional Materials》 2010-S1
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Adsorption properties of 8-hydroxyquinoline chelating resin based on phenolic resin skeleton

CHANG Huai-chun,SONG Nan-nan,SUN Qing-feng,XU Qiu-ju,JIANG Yu-chun,HAN Guang-xi,ZHANG Yu-yang(College of Chemistry,Liaoning University,Shenyang 110036,China)  
A new chelating resin with phenol formaldehyde resin as skeleton and 8-hydroxyquinoline as functional group was synthesized through the Friedel-Crafts reaction,in which 1,4-bis(chloromethoxy) butane(BCMB),phenol formaldehyde resin(PF) and 8-hydroxyquinoline are as raw material.The name of the chelating resin is abbreviated as PF-HQ.Adsorption capacity and adsorption selectivity of the PF-HQ chelating resin for different metal ions are studied.The adsorption properties of the PF-HQ chelating resin for Cu2+ and Pb2+ ions are studied by the static method.The experimental results show that the adsorption isotherm process accorded with Freundlich models.In addition,the adsorption kinetics of the PF-HQ resin also suggests the accordance with Boyd film diffusion equation.Breakthrough points of Cu2+ and Pb2+ on PF-HQ column are 22nd bed volume and 17th bed volume respectively under dynamic condition.It is good to use 5mol/L nitric acid for removing Cu2+ and Pb2+ irons.It is found that both the rate of desorption for removing over 96% the Cu2+ and Pb2+ ions respectively adsorbed on PF-HQ are 3 bed volumes.The PF-HQ resin has good eluted properties.
【Fund】: 辽宁省自然科学基金资助项目(20082049)
【CateGory Index】: TQ425.2
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