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《Journal of Functional Materials》 2013-04
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Synthesis and characterization of hyperbranched collagen fiber absorbent

WANG Xue-chuan,ZHANG Fei-fei,QIANG Tao-tao(Key Laboratory of Chemistry and Technology for Light Chemical Industry,Ministry of Education, Shaanxi University of Science and Technology,Xi'an 710021,China)  
Cr(Ⅵ) is one of contaminants in the industrial wastewater under strict control of pollution.This study used glutaraldehyde as crosslinking agent to graft hyperbranched polyamide amine(HPBN) onto collagen fiber(CF) to prepare hyperbranched collagen fiber absorbent(CF-HBPN).The influence of different conditions on the treatment effect was studied by the amino group content of CF-HBPN.IR,DSC-TGA,SEM-EDS were used to characterized the structure of product.The experimental results indicated that the optimum reaction conditions on the preparation of absorbent were the quality ratio of collagen fiber and HBPN was 1∶0.7,the dosage of crosslinking agent was 0.533mL/gCF,the temperature was 40℃,4h.Under these conditions,the amino content of CF-HBPN was 3.27 times higher than that of CF.Moreover,the absorbent prepared under these conditions was used in the treatment of solution contain Cr(Ⅵ),the removal rate was 99.57%.
【Fund】: 国家自然科学基金资助项目(21076120);; 陕西省教育厅科技计划资助项目(12JK0594);; 咸阳市科技计划资助项目(2011K10-11);; 西安市未央区科技计划资助项目(201118)
【CateGory Index】: X703.5
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