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《Journal of Functional Polymers》 2005-01
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Study on the Molecular Imprinted Polymers with Recognition Properties Towards to Dibenzoyl-L-tartaric Acid Prepared by Photo-Polymerization Method Ⅰ. Photo-polymerization Conditions

YANG Zuo-guo, XU Zhen-liang(Chemical Engineering Research Center, East China Univesity of Science and Technology, Shanghai 200237,China)  
Using a functional monomer(methyl methacrylate, acrylamide, ethyl acrylate or acrylic acid) and a crosslinker(TMPTA), molecularly imprinted polymers(MIPs) with recognition properties to dibenzoyl-L-tartaric acid(L-DBTA) were prepared by photopo-polymerization method in the presence of a template(L-DBTA) in acetonitrile solution.The experimental results indicated that the MIPs had higher L-DBTA binding ability than D-DBTA′s and also higher than corresponding non-imprinted polymers. The binding ability of MIPs is the highest at template (n_(L-DBTA)/n_(AA)/n_(TMPTA)= 1/4/12 as photo-polymerization time was 1.5h and photopolymering in a ice-water bath under a 100W ultraviolet lamp about 0.07m. Based on the optimal experimental results, it was found that the highest separation factor (α) of L-DBTA/D-DBTA of the MIPs could reach to be 5.41.
【Fund】: 国家重点基础研究发展计划(973计划)资助(2003CB615705)
【CateGory Index】: TQ316.3
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