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《Journal of Functional Polymers》 2007-03
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Molecularly Imprinted Chitosan Membrane for Chiral Resolution of Phenylalanine Isomers

WU Hong,ZHAO Yan-yan,YU Ying-xia,JIANG Zhong-yi(Key Laboratory for Green Chemical Technology,School of Chemical Engineering and Technology,Tianjin University,Tianjin 300072,China)  
Molecularly imprinted chitosan(CS) membranes were prepared by phase inversion process using CS as bulk polymer,and L-phenylalanine (L-Phe) as imprinting molecules.Two post-treatment methods including alkaline treatment and sulphuric acid crosslinking are applied to reduce the membranes' swelling capacity and then to maintain the stereo structure of the imprinting molecule cavities.FT-IR and SEM were used for membrane characterization.The chiral separation ability of the CS molecularly imprinted membranes towards the D,L-Phe aqueous mixture was evaluated by permeation experiments.Compared with the control CS membrane,an improved selectivity with a separation factor (α_(D/L)) of 1.43 is achieved.
【Fund】: 国家自然科学基金(20306021)
【CateGory Index】: TQ028.8
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