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《Chinese Journal of Spectroscopy Laboratory》 2009-02
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Synthesis and Luminescent Properties Analysis of CaO-SiO_2-B_2O_3:Pr~(3+) Glasses

SHI Peng-Tu a,b CHENG Yi-Min a XIONG Xiao-Su a CHEN Hong-Jun a SHU Wan-Gen ba(Hunan Province Product Commodity Quality Supervision Testing Institute,Changsha 410007,P.R.China)b(College of Chemistry and Chemical Engineering,Central South University,Changsha 410083,P.R.China)  
CaO-SiO2-B2O3:Pr3+ glasses were synthesized in air atmosphere with conventional high temperature process.The optimal temperature of synthesis,the structure of network and the luminescent properties of the glasses were studied.The fluorescence spectrum of Pr3+ is observed in CaO-SiO2-B2O3:Pr3+ glasses.The fluorescence spectrum of the sample has five major emission bands peaking at 480nm,532nm,546nm,605nm and 663nm respectively.The strongest emission band peaks at 603nm.The emission bands peaking at 480nm,532nm,546nm,605nm and 663nm correspond to the 3P1-3H4 transition,3P1-3H5 transition,3P1-3H4 transition,3P0-3H6 transition and 3P1-3H3 transition respectively.The study on the effect of the concentration of Pr3+ shows that there is concentration quenching phenomenon in the glasses.The luminescent properties of CaO-SiO2-B2O3:Pr3+ glasses indicate that the glass can convert the ultraviolet in the sunlight into red light,thus increasing the intensity of red light.We can take advantage of the luminescent properties of these glasses to make kinds of light-conversion glass for agriculture.
【Fund】: 湖南省自然科学基金资助项目(02JJY2020)
【CateGory Index】: TQ171.1
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