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《Chinese Journal of Spectroscopy Laboratory》 2011-06
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Determination of Trace Cadmium by Differential Pulse Stripping Voltammetry with Bismuth Film Electrode

HAN Jun-Feng(Department of Chemistry and Chemical Engineering,Mudanjiang Teachers College,Mudanjiang,Heilongjiang 157012,P.R.China)  
A novel differential pulse stripping voltammetry for the determination of cadmium at bismuth film electrode(BFE)was investigated,and several experiential parameters were optimized.Compared with the mercury film electrode,the bismuth film electrode could yield an equally well-defined and sharp stripping signals for Cd(Ⅱ).In addition,the bismuth film electrode had a highly excellent reproducibility for detection.The bismuth film electrode exhibited highly linear behavior in the examined concentration range from 10μg·L-1 to 440μg·L-1 of Cd(Ⅱ) with the detection limit of 4.66μg·L-1 Cd(Ⅱ).The favorable performance obtained at bismuth film electrode coupled with the negligible toxicity of bismuth made the bismuth film electrode extremely attractive for environmental and industrial measurements of cadmium.
【Fund】: 牡丹江师范学院科学技术研究项目(KZ201001);; 黑龙江省自然科学基金项目(13201016)
【CateGory Index】: O657.14;O614.242
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