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《Chinese Journal of Spectroscopy Laboratory》 2012-03
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Rapid Determination of Icariin and Epimedin C in Epimedium by Near Infrared Spectroscopy

YU Xiao-Xue YI Yin a ZHOU Ning b FENG Ze-Xi b WU Qing(Key Laboratory for Information System of Mountainous Area and Protection of Ecological Environment of Guizhou Province,Guiyang 550001,P.R.China)a(College of Life Sciences,Guizhou Normal University,Guiyang 550001,P.R.China)b(Cuizhou Tongjitang Pharmaceutical Co.,Ltd,Guiyang 550002,P.R.China)  
The contents of the active constituents icariin and epimedin C in epimedium were rapidly,simultaneously and quantificationally analyzed based on the near infrared spectroscopy(NIR),and the mathematical calibration model between near infrared spectrum information and prediction components was established by partial least square(PLS).The results showed that the spectra were pretreatments by standard normal variable conversion(SNV) and first derivative,and the established calibration models of icariin and epimedin C had the optimal effects.The RMSEC(standard deviation of the calibration sets) of icariin and epimedin C were respectively 0.217and 0.718,and correlation coefficient were 0.9825 and 0.9863,respectively,RMSEP(standard deviation of the prediction sets) were 0.155 and 0.297,respectively.The method is simple,accurate,that can be more suitable to rapidly analyze major compositions in epimedium medincinal materials.
【Fund】: 国家863计划项目(2009AA043201);; 国家科技重大专项项目(2009ZX09313-034)
【CateGory Index】: O657.33;R284
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