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《Journal of Lanzhou University of Technology》 2007-05
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Synthesis of chloro[tris(2-aminoethyl)amine]zinc(II) tetrafluoroborate,{[(tren)ZnCl]BF_4} and its crystal structure

QIAN Bao-hua,MA Wei-xing (Dept.of Chemical Technology,Huaihai Institute of Technology,Lianyungang 222005,China)  
A new mononuclear complex {[(tren)ZnCl]BF4} was synthesized based on the reaction of zinc chloride,sodium tetrafluoroborate and tren(tris(2-aminoethyl) amine) in methanol medium.Its structure was characterized with IR spectrum,1H NMR.The crystal structure of the compound was also determined with X-ray mono-crystal diffraction.The crystal was of monoclinic system with space group P2(1)/c,and crystallographic data of the compound were a=1.068 0(3) nm,b=1.153 2(3) nm,c=1.103 4(3) nm,α=90.00°,β=102.453°,γ=90.00°,V=1.327 0(7) nm3,Dc=1.671 g/cm3,Z=4,F(000)=680, μ=2.083 mm-1.
【CateGory Index】: O627.2
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【References】
Chinese Journal Full-text Database 1 Hits
1 MA Wei-xing1,QIAN Bao-hua1,GE Hong-yu1,XU Xing-you1,LU Lu-de2(1.School of Chemical Engineering,Huaihai Institute of Technology,Lianyungang 222005,China;2.Materials Chemistry Laboratory,Nanjing University of Science & Technology,Nanjing 210094,China);Synthesis,Characterization,Crystal Structure of Acetate Bridged Complex {[(tren)Zn(CH_3COO)Zn(tren)](BF_4)_3}[J];Journal of Synthetic Crystals;2009-03
【Citations】
Chinese Journal Full-text Database 1 Hits
1 MA Wei-Xing1,2 QIAN Bao-Hua1,2 GAO Jian1 XU Xing-You1,2 LU Lu-De*,1YANG Xu-Jie1 WANG Xin1 SONG Hai-Bin3(1Materials Chemistry Laboratory, Nanjing University of Science & Technology, Nanjing 210094)(2Dept. of Chemical Technology, Huaihai Institute of Technology, Lianyungang 222005)(3College of Chemistry, Nankai University, Tianjin 300071);Synthesis, Crystal Structure and Spectral Characterization of the Complex [Zn(Tren)(H-SSA)][J];Chinese Journal of Inorganic Chemistry;2005-04
【Co-citations】
Chinese Journal Full-text Database 5 Hits
1 QIAN Bao-hua1,2,MA Wei-xing2,LI Shan-zhong1,2,XU Xing-you1,2,LU Lu-de1,,YANG Xu-Jie1,WANG Xin1 (1.Materials Chemistry Laboratory,Nanjing University of Science & Technology,Nanjing 210094,China;2.Department of Chemical Technology,Huaihai Institute of Technology,Lianyungang 222005,China);Synthesis,characterization and crystal structure of tris-(propane-1,2-diamino-N,N′)zinc(Ⅱ) perchlorate complex[J];Chemical Reagents;2008-09
2 HUANG Xu-jun(Hunan Industrial Vocation Technology College,Chenzhou Hunan 42300,China);Hydrothermal Synthesis and Crystal Structure of the Complex Zn(phen)_2[(C_6H_5)_2C(OH)COO]_2[J];Journal of Hengyang Normal University;2008-03
3 QIAN Bao-hua1,2,MA Wei-xing2,LI Shan-zhong1,2,XU Xing-you1,2,LU Lu-de1,YANG Xu-jie1,WANG Xin1 (1.Materials Chemistry Laboratory,Nanjing University of Science and Technology, Nanjing 210094,China;2.Department of Chemical Technology,Huaihai Institute of Technology,Lianyungang 222005,China);Synthesis,Characterization and Structure of Formic Acid Bridged Binuclear Zn(II) Complex[J];Journal of Synthetic Crystals;2007-06
4 WANG Jian1 2,XU Xing-you1 2,MA Wei-xing1,ZHAO Hong1,LU Lu-de2,YANG Xu-jie2,WANG Xin2(1.Huaihai Institute of Technology,Lianyungang 222005,China;2.Materials Chemistry Laboratory,Nanjing University of Science and Technology,Nanjing 210094,China);Synthesis of [Zn(L-trp)(D-trp)]_n by Mixed Solvent-thermal Method[J];Journal of Synthetic Crystals;2008-05
5 MA Wei-xing1,QIAN Bao-hua1,GE Hong-yu1,XU Xing-you1,LU Lu-de2(1.School of Chemical Engineering,Huaihai Institute of Technology,Lianyungang 222005,China;2.Materials Chemistry Laboratory,Nanjing University of Science & Technology,Nanjing 210094,China);Synthesis,Characterization,Crystal Structure of Acetate Bridged Complex {[(tren)Zn(CH_3COO)Zn(tren)](BF_4)_3}[J];Journal of Synthetic Crystals;2009-03
【Co-references】
Chinese Journal Full-text Database 8 Hits
1 MA Wei-xing~(1,2),QIAN Bao-hua~(2,3),CHENG Qing-fang~2,WANG Jian~(2,3),XU Xing-you~(2,3)LU Lu-de~3,YANG Xu-jie~3,WANG Xin~3,SONG Hai-bin~4(1.Jiangsu Provincial Key Laboratory of Ocean Biotechnology,Huaihai Institute of Technology,Lianyungang 222005,China;2.Department of Chemical Technology,Huaihai Institute of Technology,Lianyungang 222005,China;3.Materials Chemistry Laboratory,Nanjing University of Science and Technology,Nanjing 210094,China;4.College of Chemistry,Nankai University,Tianjin 300071,China);Synthesis,Crystal Structure and Spectral Characterization of the Complex [Zn(CH_3COO)_2(C_7H_6N_2S)_2][J];Journal of Synthetic Crystals;2006-05
2 MA Wei-xing~(1,2),QIAN Bao-hua~2,CHEN Jun~2,SHA Ou~2,XU Xing-you~2 (1.Jiangsu Provincial Key Laboratory of Ocean Biotechnology,Huaihai Institute of Technology,Lianyungang 222005,China;2.Department of Chemical Engineering,Huaihai Institute of Technology,Lianyungang 222005,China);Synthesis,Crystal Structure and Spectral Characterization of the Complex[Zn(CH_3CH_2CH_2CH_2N=CHC_6H_4O)_2][J];Journal of Synthetic Crystals;2006-06
3 ZHAO Guo-Liang* FENG Yun-Long LIU Xing-Hai(College of Chemistry and Life Science, Zhejiang Normal University, Jinhua 321004);Synthesis, Characterization,Crystal Structure and Kinetics of Thermal Decomposition of Zn(Ⅱ) Complex[J];Chinese Journal of Inorganic Chemistry;2005-04
4 MA Wei-Xing1,2 QIAN Bao-Hua1,2 GAO Jian1 XU Xing-You1,2 LU Lu-De*,1YANG Xu-Jie1 WANG Xin1 SONG Hai-Bin3(1Materials Chemistry Laboratory, Nanjing University of Science & Technology, Nanjing 210094)(2Dept. of Chemical Technology, Huaihai Institute of Technology, Lianyungang 222005)(3College of Chemistry, Nankai University, Tianjin 300071);Synthesis, Crystal Structure and Spectral Characterization of the Complex [Zn(Tren)(H-SSA)][J];Chinese Journal of Inorganic Chemistry;2005-04
5 MA Wei-Xing1,2 GAO Jian1 QIAN Bao-Hua1,2 XU Xing-You1,2 LU Lu-De*,1 YANG Xu-Jie1 WANG Xin1 SONG Hai-Bin3 (1Materials Chemistry Laboratory, Nanjing University of Science & Technology, Nanjing 210094) (2Dept. of Chemical Technology, Huaihai Institute of Technology, Lianyungang 222005) (3College of Chemistry, Nankai University, Tianjin 300071);Synthesis, Crystal Structure and Spectral Characterization of Coordination Polymer{[Zn(CF_3COO)_2(C_5H_5ON)·]H_2O}_n[J];Chinese Journal of Inorganic Chemistry;2005-05
6 XU Xing-You*,1,2 GAO Jian2 CHEN Jun1,3 LI Shan-Zhong1,2 YANG Xu-Jie2 LI Yi-Zhi3 LIU Yong-Jiang3 (1Department of Chemical Engineering, Huaihai Institute of Technology, Lianyungang 222005) (2Materials Chemistry Laboratory, Nanjing University of Science & Technology, Nanjing 210094 ) (3State Key Laboratory of Coordination, Coordination Chemistry Institute, Nanjing University, Nanjing 210093);Synthesis, Structure and Antimicrobial Study of N-salicylidene-benzylamineato Transition Metal Complexes[J];Chinese Journal of Inorganic Chemistry;2005-05
7 MA Wei-Xing*,1,2 QIAN Bao-Hua2,3 LI Shan-Zhong2,3 WANG Jian2,3 XU Xing-You2,3 LU Lu-De3 SONG Hai-Bin4 (1Jiangsu Provincial Key Laboratory of Ocean Biotechnology, Huaihai Institute of Technology, Lianyungang, Jiangsu 222005) (2Dept. of Chemical Technology, Huaihai Institute of Technology, Lianyungang, Jiangsu 222005) (3Materials Chemistry Laboratory, Nanjing University of Science & Technology, Nanjing 210094) (4College of Chemistry, Nankai University, Tianjin 300071);Synthesis, Crystal Structure and Spectral Characterization of the Complex [Zn(CF_3COO)_2(C_7H_6NS)_2][J];Chinese Journal of Inorganic Chemistry;2006-10
8 MA Wei-Xing,1 QIAN Bao-Hua1 GE Hong-Yu1 XU Xing-You1 LU Lu-De2(1Dept.of Chemical Technology,Huaihai Institute of Technology,Lianyungang,Jiangsu 222005)(2Materials Chemistry Laboratory,Nanjing University of Science & Technology,Nanjing 210094);Synthesis,Crystal Structure and Spectral Characterization of the Complex [Zn(C_6H_5COCHCOCF_3)_2(C_5H_4NOH)][J];Chinese Journal of Inorganic Chemistry;2007-12
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