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Preparation of Nanocrystalline Titania Powders by Hydrothermal Precipitation

Huang Hui Luo Hongjie Yang Ming (Department of Materials Science and Engineering,Northwest Institute of Light Industry,Xianyang 712081) Liu Jiang (Xianyang Research and Design Institute of Ceramics,Xianyang 712081)  
Nanocrystalline anatase titania powders were prepared by hydrothemal treatment of a mixed solution of Ti(SO 4) 2(0 5M)and urea The crystal phase,grain size and morphology of the prepared powders were studied by XRD,TEM and DTA techniques The influences of [Ti(SO 4) 2]/[Urea],temperature and soaking time were discussed in details The prepared TiO 2 powders are anatase with 10~20nm in diameter under the conditions of the ratio [Ti(SO 4) 2]/[Urea]=1∶2~1∶4 and 140~200℃ for 2~6hours The experiment shows that the grain size increases with the decrease of the molar ratio [Ti(SO 4) 2]/[Urea], rise in reaction temperature and prolongation of soaking time
【CateGory Index】: O614
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