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《Bulletin of the Chinese Ceramic Society》 2009-05
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Preparation and Photocatalytic Properties of Mo-doped TiO_2

CHEN Gui-hua1,YAN Rui-qiang1,LIANG Hua-ding1,YANG Hui2(1.School of Pharmaceutical and Chemical Engineering,Taizhou University,Linhai 317000,China;2.School of Materials Science and Engineering,Zhejiang University,Hangzhou 310027,China)  
The pure TiO2 and Mo-doped TiO2 nanoparticles were prepared by Sol-gel method with tetrabutyl titanate as raw material and characterized by XRD,UV-VIS and XPS.The photocatalytic activity was investigated by degradation of methylene blue.Effects of calcined temperature and doping content of Mo on crystal lattice distortion,grain size,crystal phase,optical properties and photocatalytic activities were investigated.The results show that most of Mo6+ takes the place of Ti4+ in the crystal lattice of TiO2,which leds to distortion of crystal lattice,restrains the increase of grain size and inhabits the phase transformation from anatase to rutile of TiO2.Exciation wavelength red shift more with doping more Mo content calcined at 450 ℃.The content of anatase phase in 1.8%Mo-TiO2 mixed crystal calcined at 600 ℃,and inducing exciation wavelength blue shift.Doping with the appropriate content of Mo improves the photocatalytic activity of TiO2,the photocatalytic activity of 1.8%(in mole)Mo doped TiO2 nanoparticles is optical calcined at 600 ℃.
【Fund】: 浙江省科技计划(No.2006C11114)资助
【CateGory Index】: O643.36
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