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《Bulletin of the Chinese Ceramic Society》 2012-06
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Preparation of Mono-disperse SiO_2 Nano-spheres by a Non-ionic Reverse Micellar System

HAN Qun,WU Li-hua,CHEN Jing,DING Shi-jie(School of Life Science and Chemical Engineering,Jiangsu Provincial Key Laboratory of Palygorskite Science and Applied Technology, Huaiyin Institute of Technology,Huaian 223003)  
The preparation of nanosized,monodisperse silica particles by controlled hydrolysis of tetraethoxysilane(TEOS) in a non-ionic surfactant/cyclohexane/ammonium hydroxide reverse micellar system is described.The results analyzed with SEM,TEM and DLS show that the size and its polydispersity of the prepared silica nanoparticles can be well controlled by changing some parameters such as the water to surfactant molar ratio(R),the concentration of ammonium hydroxide,and the water to TEOS molar ratio(h).
【Fund】: 国家自然科学基金资助项目(Grant No.21174046 51174096)
【CateGory Index】: TB383.2;TQ127.2
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