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《Spectroscopy and Spectral Analysis》 1989-01
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DETERMINATION OF As,Sb and Bi IN GEOCHEMICAL SAMPLES BY HYDRIDE GENERATION-AAS

Zhang Peiyu Reseach Institute of Geology for Mineral Resources, CNNC Guilin  
A rapid, simple and sensitive method for the determination of As, Sb and Bi in geochemical samples by hydride generation-AAS with an electrically heated quaritz tube has been stduied in this paper. The optimum conditions and the interference from 46 foreign ions were discussed potassium iodide, ascorbic acid, thiourea and phenanthroline were chosen as the interference supprressing agents. The characteristic concentration(ng/ml per 1%) and relative standard deviation of As, Sb, Bi are 0.083 and 3.77% (for 18 ppm As), 0.090 and 2.94% (for 2ppm Sb), 0.088 and 7.22%(for 0.8ppm Bi), respe ctively.
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