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《Spectroscopy and Spectral Analysis》 2002-05
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Determination of Lead in Grape Wine by Graphite Furnace Atomic Absorption Spectrometry with Ammonium Dihydric Phosphate as Modifier

ZUO Zheng-yun 1,ZHANG Min 2,SUN Zhi-an 1,and WANG De-shu 2 1.Tongling Entry-Exit Inspection and Quarantine Bureau,Tongling 244000,China 2.Tongling Environmental Monitoring Station,Tongling 244000,China  
Ammonium dihydric phosphate (NH 4H 2PO 4),palladium chloride,nickelous nitrate and mgnesium nitrate were used as modifiers respectively, to directly detect lead in grape wine with graphite furnace atomic absorption spectrometry(GFAAS).The results showed that NH 4H 2PO 4 might be the best modifier .It was found that the organic matter in grape wine interfere with the determination.To remove the interference and detect lead directly with GFAAS,not only did samples need to be diluted with 4 to 10 times sample volumes of de-ionized water,but also the standard addition method was used.The method had good precision and accuracy when concentration of lead was above 10 μg·L -1,the relative standard deviations of lead were between -5.4% and 6.2%.
【CateGory Index】: O657.3
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