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《Spectroscopy and Spectral Analysis》 2007-05
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TLC-SERS Study on Evodiamine in Evodia Rutaecarpa

ZHANG Jin-zhi1, WANG Yuan2, CHEN Hui2, SHAO Hui-bo21. North University of Technology, Beijing 100041, China2. Department of Chemistry, Capital Normal University, Beijing 100037, China  
A new method for analyzing the ingredients of evodiamine(EV), rutaecarpine(RU), hydroxyevodiamine(HYD), evodiamide(ED), dihydrorutaecarpine(DRU) and 14-formyldihydrorutaecarpine(FDRU)in evodia rutaecarpa using high performance thin layer chromatography (TLC) and surface enhanced Raman spectroscopy (SERS) technique is reported. The character of this method is that standard samples are not needed . The results show that the characteristic spectral bands of EV, RU, HYD, and ED can be obtained from the TLC spot with microgramme of sample. The spectral band at 1 562 cm-1 was obtained with great enhancement. Molecule absorbed in surface silver sol by π electrons in ring. The spectral bands of EV, RU, HYD and ED are obviously different due to their differences in structure. The TLC and SERS techniques standard samples are a convenient and speedy method to analyze chemical ingredients with high sensitivity for the study of the Chinese traditional medicine.
【Fund】: 国家自然科学基金项目(29973026)资助
【CateGory Index】: R284
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