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《Trace Elements Science》 2005-01
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Determination of Total Iron in Environmental Water

YANG Li-zhu,YANG Xin-yu,XIE Xia-feng,YANG Xiao-feng,QIU Pei-hong (School of Pharmacy,Wenzhou Medical College,Wenzhou 325027,China)  
In 0.04 mol/L NH 3·H 2O-NH 4Cl buffer solution,at pH 8.5,a sensitive second derivative polarographic wave of Fe-MTB-NO 2 - complex appears at -1.10V(vs.SCE).The peak current is proportional to iron concentration in the range of 3.0×10 -8～5.0×10 -6 mol/L,the detection limit is 1.0×10 -8mol/L.Several electrochemical methods have been used to study the properties of the polarographic wave.It is proved that the wave is a catalytic adsorptive one.The molar ratio of Fe(Ⅱ)to MTB is 1∶1.This method has been successfully applied to the determination of trace total iron in water samples.
【CateGory Index】： X832
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