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《Guangxi & Development of Chemical Industry》 2005-02
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Determination of Apigenin in Marchantia Convoluta

ZHU Hua~1,ZOU Deng-feng~1,HUANG Hai-bin~1,XIAO Jian-bo~2,LIU Guang-tian~2(1.Guangxi Chinese Medicine University,Nanning 530001,China;2.College of Chemistry and Chemical Engineering,Central South University,Changsha 410083,China)  
A method for determination of apigenin in Marchantia convoluta was established. The sample was extracted by 80% ETOH,then the solution was purified through the solid phase extraction column with silica gel as stationary phase. The liquid which was eluted after the cartridge absorbed apigenin to saturation state was used as a test solution and measured by HPLC-UV. The proposed method can overcome the drawback of incomplete extraction of apigeninfor conventional liquid-liquid extraction method. The linear range of 1.60~12.80 mg/L(r=0.9995),recoveries of 96.93 %~106.12 % and RSD of 1.6 %(n=5) for the method were obtained. The method was proved to be simple,accurate,repeatable,and could be used for the quality control of apigenin in Marchantia convoluta.
【Fund】: 广西区科技攻关项目 ;桂科攻 0 2 35 0 2 2 - 1B;; 广西区回国人员科技基金项目 ;桂科回 0 0 0 90 0 4
【CateGory Index】: R284
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