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《Guangxi & Development of Chemical Industry》 2005-02
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Determination of Apigenin in Marchantia Convoluta

ZHU Hua~1,ZOU Deng-feng~1,HUANG Hai-bin~1,XIAO Jian-bo~2,LIU Guang-tian~2(1.Guangxi Chinese Medicine University,Nanning 530001,China;2.College of Chemistry and Chemical Engineering,Central South University,Changsha 410083,China)  
A method for determination of apigenin in Marchantia convoluta was established. The sample was extracted by 80% ETOH,then the solution was purified through the solid phase extraction column with silica gel as stationary phase. The liquid which was eluted after the cartridge absorbed apigenin to saturation state was used as a test solution and measured by HPLC-UV. The proposed method can overcome the drawback of incomplete extraction of apigeninfor conventional liquid-liquid extraction method. The linear range of 1.60~12.80 mg/L(r=0.9995),recoveries of 96.93 %~106.12 % and RSD of 1.6 %(n=5) for the method were obtained. The method was proved to be simple,accurate,repeatable,and could be used for the quality control of apigenin in Marchantia convoluta.
【Fund】: 广西区科技攻关项目 ;桂科攻 0 2 35 0 2 2 - 1B;; 广西区回国人员科技基金项目 ;桂科回 0 0 0 90 0 4
【CateGory Index】: R284
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5 CAO Hui1, XIAO Jian-bo 1,*, ZHOU Chun-shan1, ZHANG Yi-wei2 (1.College of Chemistry and Chemical Engineering, Central South University, Changsha 410083, China; 2. Institute of Clinical Pharmacology, Central South University, Changsha 410078, China);Comparison of Gas Chromatography-Mass Spectrometry Analysis in Different Extract Parts of Marchantia convoluta and Study on Partial Biologic Activity[J];Journal of Chinese Mass Spectrometry Society;2005-01
Chinese Journal Full-text Database 10 Hits
1 NIU Yan et al (College of Life Sciences and Key Laboratory of Resource Biology and Biotechnology in Western China,Ministry of Education,Northwest University,Xian,Shaanxi 710069);Research on the Distribution of Bryophytes in Cuihua Mountain[J];Journal of Anhui Agricultural Sciences;2008-34
2 RU Xin et al(Tianjin Museum of Natural History,Tianjin 300074);Investigations of Bryoflora in Tianjin Baxianshan National Nature Reserve[J];Journal of Anhui Agricultural Sciences;2009-03
3 WANG Wen-he~(1a),YU Tong-quan~(2),XU Hong-mei~(1b),ZHANG Li-zhen~(1a)(1.a.Department of Landscap;b.Editorial Office of Journal,Beijing Agricultural College,Beijing 102206,China;2.Beijing Key Laboratory New Technology in Agriculture Application,Beijing 102206,China);Study on Bryophyte in JiuFeng's National Forest Park[J];Journal of Beijing Agricultural College;2006-02
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【Secondary References】
Chinese Journal Full-text Database 5 Hits
1 LU Wan-ping1,YOU Fei-ming2,LI Xin1,WU Fang1,ZHANG Lan1(1.Instrumentation Analysis and Measurement Center of Fuzhou University,Fuzhou 350002;2.Fu jian Provincial Central Inspection Institute,Fuzhou 350002,China);Study on Pretreatment Method for Determination of Organochlorine and Pyrethroid Pesticides Residues in Teas[J];Analysis and Testing Technology and Instruments;2009-02
2 SU Jian-feng,HU Chao-yang,CHEN Jin-xing and CHEN Pei-gui(Fujian Fairreach Food Safety Testing Co.,Ltd,Fuzhou 350015);Rapid determination of residual amounts of 103 pesticides in green soy bean by gas chromatography/mass spectrometry[J];Chinese Journal of Analysis Laboratory;2009-06
3 ZHENG Xiao-yan1,LU Wan-ping2,HUANG Hong-xia1,CHEN Jin-quan2,ZHANG Lan2(1Fu jian Provincial Central Inspection Institute,Fuzhou 350002,China;2.Instrumentation Analysis and Measurement Center of Fuzhou University Fuzhou 350002,China);Solid Phase Extraction GC Analysis of Phosphate Pesticide Residue in Vegetables and Fruits[J];Analysis and Testing Technology and Instruments;2009-03
4 ZHOU Fang, SUN Cheng, LIU Hao;Research on Operation Improvement of Solid Phase Extraction[J];Jiangsu Environmental Science and Technology;2008-01
5 CHEN Meng,LU Wan-qing,HAN Yan,HUANG Qun-teng,SUN Guang-da(Environmental Science Research Center,College of Oceanography and Environment,Xiamen University,Xiamen 361005,China);Simultaneous Determination of 36 Pesticides in River Water and Sea Water Using Solid Phase Extraction-Gas Chromatography[J];Journal of Instrumental Analysis;2009-12
【Secondary Citations】
Chinese Journal Full-text Database 8 Hits
1 Li Meiqing 1, Sheng Xuan 2, Shao Xueguang *1 1(Department of Chemistry, University of Science and Technology of China, Hefei 230026) 2(Anhui Entry-Exit Inspection and Quarantine Bureau, Hefei 230061);Separation and Determination of Active Components of Pueraria Lobata Isoflavonoid Extract by Reversed Phase High Performance Liquid Chromatography[J];Chinese Journal of Analytical Chemistry;2003-02
2 Zhang Dan  (School of Pharmacy, Sichuan University, Chengdu 610041) Jiang Xinhui (Department of Pharmacy, Chongqing University of Medical Sciences, Chongqing 400016);Determination of Aloe-emodin, Rhein, Emodin and Chrysophanol in Radix Rhei by Reversed Phase High Performance Liquid Chromatography[J];Chinese Journal of Analytical Chemistry;2003-04
3 ZHU Hua a,b XIAO Jian Bo a ZHONG Shi An a ZHOU Chun Shan a REN Xiu Lian a a(College of Chemistry and Chemical Engineering,Central South University,Changsha 410083,P.R.China) b(Guangxi Chinese Medical University,Nanning 530001,P.R.China);Determination of Flavonoids in Marchantia Poymorpha[J];Chinese Journal of Spectroscopy Laboratory;2004-02
4 LUO Weiqiang1 ,HUANG Runjun2 , DENG Guanghui1 ( 1.Department of Chemistry and Chemical Engineering, Guangxi University for Nationalities,Nanning,530006,China; 2.Nanning Branch of Guilin Institute of Technology, Nanning 530001,China);Leaching Method of Flavones from Ixerischinesis (thunb) Nakai Stem[J];Journal of Guangxi University For Nationalities(Natural Science Edition);2003-01
5 LIN Chun-rui ( Guangxi Institute of Botany, Guangxi Zhuangzu Autonomous Region and The Chinese Academy of Sciences, Guilin 541006, China );The determination of flavonoid content of flowers of Chrysanthemum indicum[J];Guihaia;2002-05
6 ZHU Hua~(1,2), XIAO Jian-bo~1, ZHONG Shi-an~1, ZHOU Chun-shan~1, HUANG Hai-bing(1.College of Chemistry and Chemical Engineering,Central South University,Changsha 410083,China; 2.Guangxi Chinese Medical University,Nanning 530001,China);STUDY ON LEACHING AND PURIFYING METHOD OF FLAVONES FROM MARCHANTIA POLYMORPHA L.[J];Chemistry & Industry of Forest Products;2004-02
7 Li Weili;Study on Optimal Extraction Conditions of Flavanoids from Propolis[J];Food Science;2003-05
8 XU Yong 1, GUO Xing-jie 1, FAN Jie 2, LI Fa-mei 1 (1.School of Pharmacy, Shenyang Pharmaceutical University, Shenyang 110016, China; 2.The Centeral Hospital of Huludao, Huludao 125001, China);Studies on the process for extraction of Psoralea corylifolia L. by orthogonal experiments[J];Journal of Shenyang Pharmaceutical University;2003-02
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