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《Journal of Chemical Engineering of Chinese Universities》 2011-03
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Fabrication and Property Investigation of the Highly Ordered TiO_2 Nanotube Arrays

LAN Yu-wei1,2,ZHOU Li-ya1,2,TONG Zhang-fa1,PANG Qi3,LENG Li-ming1, HAN Jian-peng1,WANG Fan1(1.College of Chemistry and Chemical Engineering,Guangxi University,Nanning 530004,China; 2.Key Laboratory of Semiconductor Materials Science,Institute of Semiconductors, Chinese Academy of Sciences,Beijing 100083,China; 3.Department of Chemistry and Biology,Yulin Teachers College,Yulin 537000,China)  
The highly ordered and uniform TiO2 nanotube arrays were fabricated by anodic oxidation of titanium foil in ethylene glycol solution containing NH4 F.The diameter,density,length and wall thickness of the prepared nanotube arrays can be controlled effectively by varying the anodization parameters.The microstructures and morphologies of the fabricated TiO2 nanotube were characterized by scanning electron microscope(SEM) and X-ray diffraction(XRD),and its photocatalytic properties were investigated via the degradation of methyl orange.The results show that the highly ordered and uniform TiO2 nanotube arrays could be grown under the conditions optimized by authors.Using the prepared TiO2 nanotube arrays as photocatalyst and after 40 min illumination of the high voltage mercury lamp(500 W),the degradation ratio of methyl orange in its aqueous solution with concentratin of 20 mg·L-1 can reach 99.4% when the solution pH value is 2.0.And it was found that the photocatalysis of TiO2 nanotube can be improved by adding H2O2 into the solution.
【Fund】: 国家自然科学基金(20863008);; 广西大学科研基金(090005);; 中国科学院半导体研究所半导体材料科学重点实验室开放基金(KLSMS-0905)
【CateGory Index】: TB383.1
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