Full-Text Search:
Home|Journal Papers|About CNKI|User Service|FAQ|Contact Us|中文
《Journal of Guangxi University(Natural Science Edition)》 2013-03
Add to Favorite Get Latest Update

Preparation and characterization of molecularly imprinted polymers of sucrose

NING Chuen-yuan1,JIANG Lin-bin1,YUAN Xia1,LIANG Bi-chao2,YE Shao-feng2,ZHANG Yong-jun1(1.School of Chemistry and Chemical Engineering,Guangxi Key Laboratory of Petrochemical Resource Processing and Process Intensification Technology,Guangxi University,Nanning 530004,China;2.Department of Laboratory and Equipment Management,Guangxi University,Nanning 530004,China)  
The molecularly imprinted polymers have been discovered to have good selectivity for absorption.It is beneficial to separation and purification of the imprinted molecule.The molecularly imprinted polymers of sucrose were prepared by using the sucrose as template molecule,methyl methacrylate as functional monomer and N,N’-methylene bisacrylamide as crosslinker.The effects of the different initiators,dosage of initiator,dosage ratio of sugar and methyl methacrylate,reaction temperature,reaction time and the dosage ratio of functional monomer and crosslinking agent on the adsorption capacity of molecularly imprinted polymers were investigated with single factor method.The structure of imprinted polymers was analyzed by IR,SEM.The experiments showed that the optimal reaction conditions were ammonium persulfate as initiator,its concentration 1.2 mg/mL,the reaction time in 18 h,the reaction temperature at 50 ℃,the dosage ratio of methyl methacrylate and sugar in 4∶ 1,and the dosage ratio of crosslinking agent and methyl methacrylate in 5∶ 1.The SEM results showed that the molecularly imprinted polymers surface appeared crisscross network and many specific identification cavities.The FT-IR results showed that the template molecules in polymer were well eluted down.
【Fund】: 广西自然科学基金资助项目(桂科自2012GXNSFAA053028);; 广西亚热带生物资源保护利用重点实验室基金项目(SB0804);; 广西大学科研基金项目(X081089)
【CateGory Index】: O631.3
Download(CAJ format) Download(PDF format)
CAJViewer7.0 supports all the CNKI file formats; AdobeReader only supports the PDF format.
Chinese Journal Full-text Database 7 Hits
1 ZHENG Xi-ming1,2, TU Wei-ping1 (1. The School of Chemical and Energy Engineering, South China University of Technology, Guangzhou 510640, China; 2. Department of Chemistry and Environment Engineering, Wuyi University, Wuyishan 354300, China);Preparation of Monodisperse Molecularly Imprinted Polymer Beads by a Single-Step Swelling and Polymerization Method[J];Journal of Chemical Engineering of Chinese Universities;2007-01
2 WANG Tao1,HUANG Guang-jun1,WEI Yuan-an1,YAO Ping-jia2(1.College of Chemistry andChemical Engineering,Guangxi University,Nanning 530004,China; 2.College of Life Science and Technology,Guangxi University,Nanning 530005,China);Preparative separation of oligosaccharides monocomponent by polyacrylamide gel column[J];Journal of Guangxi University(Natural Science Edition);2010-03
3 LIU, Qiu-Yea LI, Wen-Youa HE, Xi-Wen*,a CHEN, Lang-Xinga ZHANG, Yu-Kui*,a,b (a Department of Chemistry, Nankai University, Tianjin 300071) (b Dalian Institute of Chemical Physics, Chinese Academy of Sciences, Dalian 116011);Study of Recognition Property of Molecularly Imprinted Bovine Hemoglobin on Surface-modified Silica Gel[J];Acta Chimica Sinica;2008-01
4 WU Wen-xiang~1,LI Li~2,LI Zhi-wei~3,YANG Geng-liang~3(1.Hebei Langfang Teachers′ College,Langfang 065000,China;2.College of Light Industry,Hebei University of Science and Engineering,Tangshan 063020,China;3.Center for Molecular Science,Research Institute of Chemistry,Chinese Academy of Sciences,Beijing 100080 China);STUDY ON THE PREPARATION AND RECOGNITION PROPERTY OF MOLECULAR IMPRINTED POLYMER OF MYCLOBUTANIL[J];Physical Testing and Chemical Analysis(Part B:Chemical Analysis);2006-02
5 Wang Rongyan~(1,2) Wang Peilong~2 Wang Jing~(2*) Wang Xichang~(1*) Zhong Yaoguang~1 (~1 College of Food Science and Technology,Shanghai Fisheries University,Shanghai 200090,China) (~2 Institute of Quality Standards and Testing Technology for Agri-Products,Chinese Academy of Agricultural Science,Beijing 100081,China);New Progress and Application of Molecular Imprinting Technique[J];Modern Scientific Instruments;2008-01
6 CAO Xi-Min,LIAO Ling,DU Li-Ming*(Center of Analysis and Test,Shanxi Normal University,Linfen 041004);Recognition Properties of Enoxacin Imprinted Polymer[J];Chinese Journal of Applied Chemistry;2008-01
7 WU Zheng-Hong(Department of Pharmaceutics,China Pharmaceutical University,Nanjing 210009,China);Application of Molecular Imprinting Technique in Pharmaceutical Science[J];Journal of China Pharmaceutical University;2005-05
Chinese Journal Full-text Database 10 Hits
1 WANG Jun et al(Geography and Environmental Science,Northwest Normal University,Lanzhou,Gansu 730070);Multi-walled Carbon Nanotubes Surface O-dichlorobenzene Preparation of Molecularly Imprinted Polymers[J];Journal of Anhui Agricultural Sciences;2011-10
2 LIU Xi1,ZHANG Zhao-Hui*1,2,ZHANG Hua-Bin1,HU Yu-Fang1,YANG Xiao1,NIE Li-Hua2 1(College of Chemistry and Chemical Engineering,Jishou University,Jishou 416000) 2(State Key Laboratory of Chemo/Biosensing and Chemometrics,Hunan University,Changsha 410082);Solid Phase Extraction of Ursolic Acid Using Imprinted Polymer Modified Multi-walled Carbon Nanotubes[J];Chinese Journal of Analytical Chemistry;2011-06
3 FANG Yan-qing,HONG Mei-hua and CHEN Yuan-tao(Department of Chemistry,Qinghai Normal University,Xining 810008);Preparation and characterization of rhein molecularly imprinted polymeric microspheres[J];Chinese Journal of Analysis Laboratory;2011-12
4 Shawket Abliz,Abdiryim Supahun,WANG Ji-de,Ismayil Nurulla College of Chemistry and Engineering,Xinjiang University,Urumqi 830046,China;Preparation of Pb~(2+) Imprinted Acrylic Acid-co-Styrene and Analysis of Its Adsorption Properties by FAAS[J];Spectroscopy and Spectral Analysis;2011-06
5 ZHENG Xi-ming1, FAN Rong-yu1, TU Wei-ping2 (1. Department of Chemistry and Environment Engineering, Wuyi University, Wuyishan 354300, China; 2. School of Chemistry and Chemical Engineering, South China University of Technology, Guangzhou 510640, China);The Relationships between Structure and Properties of Molecularly Imprinted Polymeric Microspheres[J];Journal of Chemical Engineering of Chinese Universities;2010-03
6 ZHENG Jing-jing,ZHAO Ge-ning,LI Mu-zi,XIE Wei-hong (Key Laboratory of Fermentation Engineering(Ministry of Education), Institution of Bioengineering,Hubei University of Technology,Hubei Wuhan 430068,China);The Comparison of the Different Elution Approaches in Protein Molecular Imprinting[J];Guangzhou Chemical Industry;2012-08
7 LIANG Jin-tian1,WEI Chao2,ZHENG Zhong-yi3,4,YAO Ping-jia1,WEI Yuan-an1 (1.College of Life Science and Technology,Guangxi University,Nanning 530005,China; 2.College of Chemistry and Chemical Engineering,Jiangxi Science and Technology Normal University, Nanchang 330013,China; 3.School of Chemistry and Chemical Engineering,Guangxi University,Nanning 530004,China; 4.Nanning Longchang Daily Necessities Industry Co.Ltd,Nanning 530221,China);Production of highly pure fructooligosaccharide using hemin as a mimetic catalase[J];Journal of Guangxi University(Natural Science Edition);2012-05
8 YANG Zhong;ZHANG Jing;Xinjiang Analysis and Testing Center;;Study on Preparation of Molecularly Imprinted Polymers for Gatifloxacinand[J];Guangzhou Chemical Industry;2013-17
9 YANG Zhong;ZHANG Jing;Xingjiang Analysis and Testing Center;;Simultaneous Extraction of Gatifloxacinand from Eggs Tissue by Molecularly Imprinted Matrix Solid-Phase Dispersion[J];Guangzhou Chemical Industry;2013-19
10 WANG Pan,XIONG Wei-de,ZHANG Ying-qing(College of Bioengineering,Hubei University of Technology,Wuhan 430068,China);Advance in the Molecular Imprinting Based Protein Recognition[J];Chemistry & Bioengineering;2008-09
【Secondary Citations】
Chinese Journal Full-text Database 10 Hits
1 SUN Yan-pu 1,2 YANG Wen-yuan 2 JIANG Ling 3 ( 1.College of Science, Beijing University of Chemical Technology, Beijing 100029, China; 2.College of Chemical Engineering; 3. College of Municipal Environment, Ningxia University, Yinchuan 750021, China);HPLC determination of inulin zymohydrolysis products[J];Journal of Beijing University of Chemical Technology;2003-01
2 Rong Fei~1 Li Ping~2 Yuan Chunwei~1(~1Department of Biological Science and Medical Engineering,Southeast University,Nanjing 210096,China)(~2Department of Bioengineering,Beijing University of Aeronautics and Astronautics,Beijing 100083,China);Binding characteristics of molecularly imprinted polymer for pazufloxacin[J];Journal of Southeast University (Natural Science Edition);2005-05
3 WU Xiao-feng~1,YANG Lu-hua~2 (1.Kunshan Entry-Exit Inspection and Quarantine Bureau of the People's Republic of China,Kunshan,Jiangsu,215200,China; 2.Disease Prevention and Control Center of Kunshan,Kunshan,Jiangsu,215300,China);Harms and Detecting Methods of Chloramphenicol Residue[J];Progress In Veterinary Medicine;2004-03
4 Hu Jianhua; La Xuliang; Yang Wuli; Xu Xiaojun; Fu Shoukuan(Department of Macromolecular Science);Preparation of monodisperse polymer microsphere and influence factors[J];JOURNAL OF FUDAN UNIVERSITY;1997-04
5 Zhou Jie, Han Hongyan, He Xiwen , Shi Huiming (Department of Chemistry, Nanism. University, Tianjin, 300071);Selective Enrichment and Direct Determination of Trace Drug by Solid-phase Extraction[J];Chinese Journal of Analytical Chemistry;1999-01
6 Guo Hongsheng, He Xiwen (Department of Chemistry, Nankai University, Tianjin 300071);A Study on the Binding Characteristics of Molecular Imprinted Polymer Selective for Cefalexin in Aqueous Media[J];CHINESE JOURNAL OF ANALYTIEAL CHEMISTRY;2000-10
7 Guo Hongsheng,He Xiwen,Zhou Jie (Department of Chemistry,Nankai Universtity ,Tianjin 300071) Liang Hong (College of Chemistry and Life Science,Guangxi Normal University,Guilin 541004);Characteristics of Molecular Recognition of Norfloxacin Template Polymer[J];Chinese Journal of Analytieal Chemistry;2001-02
8 Liu Qin, Zhou Yongxin, Meng Zihui, Wang Qingqing, Hu Xuying, Liu Yintang (Beijing Institute of Pharmacology and Toxicology, Beijing 100850);Determination of Nerve Agent Degradation Products in Rice by Molecule Imprinting Polymer-Solid Phase Extraction and Capillary Electrophoresis[J];Chinese Journal of Analytieal Chemistry;2001-04
9 Du Xiaoyan, Peng Tao, Li Junsuo  (College of Veterinary Medicine, Chinese Agriculture University, Beijing 100094);Preparation and Binding Characteristics of Molecularly Imprinted Polymers for Sarafloxacin[J];Chinese Journal of Analytical Chemistry;2003-06
10 Hu Xiaogang~(1,2),Li Gongke~(*1)~1(School of Chemistry and Chemical Engineering,Sun Yat-sen University, Guangzhou 510275)~2(School of Chemistry and Environment,South China Normal University,Guangzhou 510631);Application of Molecular Imprinting Technique in Sample Pretreatment[J];Chinese Journal of Analytical Chemistry;2006-07
©2006 Tsinghua Tongfang Knowledge Network Technology Co., Ltd.(Beijing)(TTKN) All rights reserved