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《China Adhesives》 2011-08
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Study on synthetic process of oxidized starch

Chen Youning,Yang Xiaoling,Zhang Zhixia(Department of Chemistry and Chemical Engineering,Xianyang Normal University,Xianyang 712000,China)  
Starch,which was used as a matrix resin of adhesive,was mainly composed of polyhydric glucose unit.The starch derivants with good performance and multi-varieties could be obtained by chemical,physical or biological deep-processing methods.An oxidized starch with CuSO4 catalyst and H2O2 oxidant was prepared.The better process conditions of preparing oxidized starch were roughly selected by single-factor experiment method.Then with pH value,oxidant content and catalyst content as experiment factors,carboxyl content in oxidized starch as evaluation index,the optimal process conditions of preparing oxidized starch were further preferred by orthogonal experiment.The results showed that the carboxyl content(0.50%) in oxidized starch was reversely maximal when reaction temperature was 45 ℃,reaction time was 2.5 h,pH value was 7,oxidant and catalyst were 20 mL and 4 mL respectively.
【Fund】: 陕西省自然科学基金资助项目(2004B13);; 咸阳师范学院专项科研基金资助项目(06XSYK105)
【CateGory Index】: TQ432.2
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