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《Journal of The Chinese Ceramic Society》 1992-01
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Xu Dichun Hao Xiaochun Zhu Xuanhui (Materials Science and Engineering Department, Tianjin University)  
By means of Raman spectroscopy, IR spectroscopy, DTA, TEM, SEM and electrokinetic method, the agglomeration control in the ultrafine ZrO_2 (Y_2O_3) powder prepared by wet chemical process has been studied. The experimental results show that during the precipitation process the electrostatic and steric effect can be intensified by high polymer additives and an uniformly dispersed colloidal suspension is obtained. After washing, the interface structure of colloidal particles of wet gel, treated by surfactant, is improved and formation of hard agglomeration in drying and calcinating is prevented. Furthermore, the effect of powder agglomeration on the properties of the fired samples is studied.
【Fund】: 国家自然科学基金
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